Journal of Inorganic Materials ›› 2024, Vol. 39 ›› Issue (6): 623-633.DOI: 10.15541/jim20230608
Special Issue: 【结构材料】陶瓷基复合材料(202409)
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Received:
2023-12-31
Revised:
2024-02-27
Published:
2024-06-20
Online:
2024-02-26
Contact:
TANG Sufang, professor. E-mail: sftang@imr.ac.cnAbout author:
ZHAO Rida (1995-), male, PhD, assistant professor. E-mail: rdzhao16s@imr.ac.cn
Supported by:
CLC Number:
ZHAO Rida, TANG Sufang. Research Progress of Ceramic Matrix Composites Prepared by Improved Reactive Melt Infiltration through Ceramization of Porous Carbon Matrix[J]. Journal of Inorganic Materials, 2024, 39(6): 623-633.
Carbon source | Density of porous carbon/(g·cm-3) | Median pore diameter of porous carbon/nm | Density of ceramic/ (g·cm-3) | Si content/% (in mass) | Ref. |
---|---|---|---|---|---|
Furfuryl alcohol | / | 1000 | / | / | [ |
Furfuryl alcohol | 0.86 | 1300 | / | / | [ |
Furfuryl | 0.74 | 2580 | 3.04 | 17.6 | [ |
0.65 | 1940 | 2.81 | 34.7 | ||
0.58 | 670 | 3.01 | / | ||
0.90 | 40 | 3.07 | / | ||
Phenol formaldehyde | 0.79 | 2363 | 2.10 | 13.0 | [ |
0.79 | 1552 | 2.81 | 12.0 | ||
0.74 | 1226 | 2.88 | 16.0 | ||
0.74 | 642 | 2.91 | 14.0 | ||
0.73 | 190 | 2.93 | 16.0 | ||
Phenol formaldehyde | 0.72 | 39.9 | 2.92 | 20.0 | [ |
0.72 | 39.9 | 3.07 | 15.4 | ||
0.79 | 28.8 | 3.08 | 12.2 | ||
0.78 | 38.7 | 2.95 | 3.1 | ||
Phenol formaldehyde | 0.90 | 20.1 | 2.90 | 3.6 | [ |
Table 1 Carbon sources, densities and median pore diameters of porous carbon, densities and Si content of obtained ceramics
Carbon source | Density of porous carbon/(g·cm-3) | Median pore diameter of porous carbon/nm | Density of ceramic/ (g·cm-3) | Si content/% (in mass) | Ref. |
---|---|---|---|---|---|
Furfuryl alcohol | / | 1000 | / | / | [ |
Furfuryl alcohol | 0.86 | 1300 | / | / | [ |
Furfuryl | 0.74 | 2580 | 3.04 | 17.6 | [ |
0.65 | 1940 | 2.81 | 34.7 | ||
0.58 | 670 | 3.01 | / | ||
0.90 | 40 | 3.07 | / | ||
Phenol formaldehyde | 0.79 | 2363 | 2.10 | 13.0 | [ |
0.79 | 1552 | 2.81 | 12.0 | ||
0.74 | 1226 | 2.88 | 16.0 | ||
0.74 | 642 | 2.91 | 14.0 | ||
0.73 | 190 | 2.93 | 16.0 | ||
Phenol formaldehyde | 0.72 | 39.9 | 2.92 | 20.0 | [ |
0.72 | 39.9 | 3.07 | 15.4 | ||
0.79 | 28.8 | 3.08 | 12.2 | ||
0.78 | 38.7 | 2.95 | 3.1 | ||
Phenol formaldehyde | 0.90 | 20.1 | 2.90 | 3.6 | [ |
Fig. 6 (a) Schematic illustration of liquid Si infiltration in double-walled carbon nanotubes, (b) relationship between infiltration height (H) and infiltration time (t) for liquid Si infiltration, and (c) capillary infiltration behavior of liquid Si into a double-walled carbon nanotubes with an inner tube diameter of 2 nm[51]
Fig. 8 (a, b) Microstructures and (c) pore size distribution curves of the porous C/C, and (d) cross-sectional micrograph of the C/C-SiC-(ZrxHf1-x)C[35]
Fig. 10 Comparison of (a) flexural strength and (b) 2200 ℃ linear ablation rates of ceramic matrix composites obtained by conventional RMI and improved RMI through ceramization of porous carbon matrix[18,33⇓-35,39]
Preform | Preparation method of porous matrix | Median pore diameter/nm | Predominant pore size range/nm | Ceramic matrix composites | Flexural strength/MPa | Ref. |
---|---|---|---|---|---|---|
C/SiC-C | Phase separation | 1800 | 500-10000 | C/SiC-Si | / | [ |
SiC/BNx/SiNx/C | Phase separation | / | 1000-4500 | SiC/BNx/SiNx/SiC-Si | / | [ |
C/B4C-C | Sol-Gel | 39800 | 25000-75000 | C/ZrB2-SiC-ZrC | 231 | [ |
C/B4C-Al2O3-C | Sol-Gel | / | 10-10000 | C/B4C-Al2O3-SiC-Si | 300 | [ |
C/ZrC-C | Carbothermal reduction | / | 4-130000 | C/ZrC-SiC-ZrSi2 | 380 | [ |
C/C | Phase separation | 41.6 | 10-80 | C/SiC | 218 | [ |
SiC/SiC-C | Phase separation | / | 100-5000 | SiC/SiC-Si | 201 | [ |
C/C | Phase separation | 1300 | 100-5200 | C/C-SiC-(ZrxHf1−x)C | / | [ |
SiC/SiC-C | Sol-Gel | / | 500-10000 | SiC/SiC-Si | 809 | [ |
C/C | Phase separation | / | 10-130 | C/SiC-ZrC | 288 | [ |
C/SiC-HfC | 251 |
Table 2 Preparation methods of porous matrix in preform, median pore diameters and predominant pore size ranges of preform, and flexural strength of the obtained ceramic matrix composites
Preform | Preparation method of porous matrix | Median pore diameter/nm | Predominant pore size range/nm | Ceramic matrix composites | Flexural strength/MPa | Ref. |
---|---|---|---|---|---|---|
C/SiC-C | Phase separation | 1800 | 500-10000 | C/SiC-Si | / | [ |
SiC/BNx/SiNx/C | Phase separation | / | 1000-4500 | SiC/BNx/SiNx/SiC-Si | / | [ |
C/B4C-C | Sol-Gel | 39800 | 25000-75000 | C/ZrB2-SiC-ZrC | 231 | [ |
C/B4C-Al2O3-C | Sol-Gel | / | 10-10000 | C/B4C-Al2O3-SiC-Si | 300 | [ |
C/ZrC-C | Carbothermal reduction | / | 4-130000 | C/ZrC-SiC-ZrSi2 | 380 | [ |
C/C | Phase separation | 41.6 | 10-80 | C/SiC | 218 | [ |
SiC/SiC-C | Phase separation | / | 100-5000 | SiC/SiC-Si | 201 | [ |
C/C | Phase separation | 1300 | 100-5200 | C/C-SiC-(ZrxHf1−x)C | / | [ |
SiC/SiC-C | Sol-Gel | / | 500-10000 | SiC/SiC-Si | 809 | [ |
C/C | Phase separation | / | 10-130 | C/SiC-ZrC | 288 | [ |
C/SiC-HfC | 251 |
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