Journal of Inorganic Materials ›› 2022, Vol. 37 ›› Issue (9): 969-975.DOI: 10.15541/jim20210771
• RESEARCH ARTICLE • Previous Articles Next Articles
LI Wenjun(), WANG Hao(
), TU Bingtian, CHEN Qiangguo, ZHENG Kaiping, WANG Weiming, FU Zhengyi
Received:
2021-12-17
Revised:
2022-02-22
Published:
2022-09-20
Online:
2022-06-16
Contact:
WANG Hao, professor. E-mail: shswangh@whut.edu.cnAbout author:
LI Wenjun (1996-), male, Master candidate. E-mail: 15826911464@163.com
Supported by:
CLC Number:
LI Wenjun, WANG Hao, TU Bingtian, CHEN Qiangguo, ZHENG Kaiping, WANG Weiming, FU Zhengyi. Preparation and Property of Mg0.9Al2.08O3.97N0.03 Transparent Ceramic with Broad Optical Transmission Range[J]. Journal of Inorganic Materials, 2022, 37(9): 969-975.
Fig. 1 Characterization of Mg0.9Al2.08O3.97N0.03 powder, slurry, green body, and transparent ceramic (a) XRD patterns of powder and ceramic; (b) Relationship between viscosity of slurry and contents of TAC; (c) Morphology of green body; (d) SEM image of etched surface of transparent ceramic
Fig. 2 Comparison of optical property of transparent ceramics (a) In-line transmittance of Mg0.9Al2.08O3.97N0.03, MgAl2O4, c-plane sapphire[1], Mg0.27Al2.58O3.73N0.27 transparent ceramics[14]; (b) Refractive index of Mg0.9Al2.08O3.97N0.03, MgAl2O4 transparent ceramics[19]
Fig. 4 Fractured strength under different load rates (a) and strength-probability-time diagram (b) of Mg0.9Al2.08O3.97N0.03 and MgAl2O4[27] transparent ceramics Colorful figures are available on website
Sample | Vickers hardness/GPa | Fracture toughness/(MPa·m1/2) | Young’s modulus/GPa | Thermal expansion coefficient/(×10-6, K-1) |
---|---|---|---|---|
MgAl2O4[ | 12.9±0.49 | 1.6±0.1 | 273 | 6.97 |
Mg0.9Al2.08O3.97N0.03 | 13.7±0.12 | 2.12±0.1 | 280 | 6.57 |
Table 1 Property of Mg0.9Al2.08O3.97N0.03 and MgAl2O4 transparent ceramic
Sample | Vickers hardness/GPa | Fracture toughness/(MPa·m1/2) | Young’s modulus/GPa | Thermal expansion coefficient/(×10-6, K-1) |
---|---|---|---|---|
MgAl2O4[ | 12.9±0.49 | 1.6±0.1 | 273 | 6.97 |
Mg0.9Al2.08O3.97N0.03 | 13.7±0.12 | 2.12±0.1 | 280 | 6.57 |
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