Journal of Inorganic Materials ›› 2020, Vol. 35 ›› Issue (7): 759-768.DOI: 10.15541/jim20190401
Special Issue: 生物材料论文精选(2020)
• REVIEW • Previous Articles Next Articles
ZHANG Xiaoxu1,2,ZHU Dongbin1,2,3(
),LIANG Jinsheng1,2
Received:2019-08-09
Revised:2019-10-02
Published:2020-07-20
Online:2020-01-20
Supported by:CLC Number:
ZHANG Xiaoxu,ZHU Dongbin,LIANG Jinsheng. Progress on Hydrothermal Stability of Dental Zirconia Ceramics[J]. Journal of Inorganic Materials, 2020, 35(7): 759-768.
Fig. 1 SEM images of zirconia microstructure (a) without and (b) with LTD, and AFM images of zirconia (c) without and (d) with LTD[17]
Fig. 2 (a) Schematic views of zirconia LTD process, and (b) oxygen vacancies of LTD mechanism[23]
Fig. 3 Theoretical model of initial dimensions and growth rate of m-ZrO2 nuclei[32] (a) Top view of surface; (b) Cross section view
Fig. 4 Ageing kinetics analysis with 3Y-TZP by μ-Raman spectroscopy[33] (a) m-ZrO2 content depth and corresponding optical images; (b)Transformed depth varies with ageing time
Fig. 5 XRD profiles for different incidence angles ω in the surface of the 3Y-TZP specimen after LTD test[37]
| Equation | |
|---|---|
| Linear | ${{V}_{\text{m}}}=\frac{I_{\text{m}}^{181}+I_{\text{m}}^{190}}{k(I_{\text{t}}^{147}+\delta I_{\text{t}}^{265})+I_{\text{m}}^{181}+I_{\text{m}}^{190}}$ Clarke and Adar[ Katagiri, et al.[ Lim, et al.[ |
| Power law[ | ${{V}_{\text{m}}}=\sqrt{0.19-\frac{0.13}{\frac{I_{\text{m}}^{181}+I_{\text{m}}^{190}}{I_{\text{t}}^{147}+I_{\text{m}}^{181}+I_{\text{m}}^{190}}-1.01}}-0.56$ |
| Logarithmic[ | ${{V}_{\text{m}}}=0.65+0.39\lg \left( \frac{I_{\text{m}}^{181}+I_{\text{m}}^{190}}{I_{\text{t}}^{147}+I_{\text{t}}^{265}+I_{\text{m}}^{181}+I_{\text{m}}^{190}} \right)$ |
Table 1 Proposed models for monoclinic phase quantification by Raman spectroscopy
| Equation | |
|---|---|
| Linear | ${{V}_{\text{m}}}=\frac{I_{\text{m}}^{181}+I_{\text{m}}^{190}}{k(I_{\text{t}}^{147}+\delta I_{\text{t}}^{265})+I_{\text{m}}^{181}+I_{\text{m}}^{190}}$ Clarke and Adar[ Katagiri, et al.[ Lim, et al.[ |
| Power law[ | ${{V}_{\text{m}}}=\sqrt{0.19-\frac{0.13}{\frac{I_{\text{m}}^{181}+I_{\text{m}}^{190}}{I_{\text{t}}^{147}+I_{\text{m}}^{181}+I_{\text{m}}^{190}}-1.01}}-0.56$ |
| Logarithmic[ | ${{V}_{\text{m}}}=0.65+0.39\lg \left( \frac{I_{\text{m}}^{181}+I_{\text{m}}^{190}}{I_{\text{t}}^{147}+I_{\text{t}}^{265}+I_{\text{m}}^{181}+I_{\text{m}}^{190}} \right)$ |
Fig. 6 SEM images of the Y-TZP ceramic[45] (a) before and (b) after LTD
Fig. 7 2Y-TZP ceramic[50] (a) SEM images together with the corresponding grain size distribution, and (b) semi-quantitative Y2O3 distribution
Fig. 8 Morphologies of samples treated with surface nitrogen after aging[60] (a) LSCM image of N-1600; (b) SEM image of N-1400; AFM images of N-1400 (c) surface and (d) bulk
Fig. 9 3Y-0.25Al ceramic[69] (a) TEM image of grain boundaries; (b) Corresponding Al elemental map
Fig.10 0.05A-TZ/SiO2 specimen images of fractured surface[74] (a) TEM image; (b) SEM image
Fig. 11 SEM images of the SWNT distribution within the 3Y-TZP/SWNT ceramic[76] (a) C1.5-UB; (b) C1.5-UP
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