Synthesis of Tungsten Oxide Nanorods Doped with Transition Metal Molybdenum

Journal of Inorganic Materials

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Synthesis of Tungsten Oxide Nanorods Doped with Transition Metal Molybdenum

CAO Guang-Sheng^1,2; YU Qing-Sen¹; DONG Xi-Gui^1,3; SONG Xu-Chun⁴; TAN Fei¹

1. Department of Chemistry; Zhejiang University; Hangzhou 310027; China; 2. Department of Petroleum Engineering; Daqing Petroleum Institute; Daqing 163318, China; 3. No. 2 Oil Production Plant of Daqing Oilfield Company Ltd.; Daqing 163414, China; 4. Department of Chemistry; Normal University of Fujian; Fuzhou 350007; China）;

Received:2004-07-05 Revised:2004-09-27 Published:2005-07-20 Online:2005-07-20

Abstract

Abstract: Tungsten oxide nanorods doped with molybdenum were synthesized by a facile hy-drothermal method using tungstenic acid precipitate doped with molybdenum as precursor, which was prepared by the reaction between HC1 solution and Na₂WO₄solution immingled different percentages of (NH₄)₆Mo₇O₂₄·4H₂0 respectively. The samples of the products were characterized by XRD, SEM, EDX, TEM and PL. The results show that the dimensions of as-synthesized tungsten oxide nanorods gradually decrease with the increase of the percentage of doped molybdenum, the photoluminescence emission peak intensities of them weaken down accordingly.

Key words: tungsten oxide, molybdenum, doping, nanorod

CLC Number:

TB383

CAO Guang-Sheng,YU Qing-Sen,DONG Xi-Gui,SONG Xu-Chun,TAN Fei. Synthesis of Tungsten Oxide Nanorods Doped with Transition Metal Molybdenum[J]. Journal of Inorganic Materials.

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Synthesis of Tungsten Oxide Nanorods Doped with Transition Metal Molybdenum

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