Synthesis of Sb Doped Tin Oxide (ATO) Nanoparticles by Complex Method

Journal of Inorganic Materials

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Synthesis of Sb Doped Tin Oxide (ATO) Nanoparticles by Complex Method

ZHANG Jian-Rong¹; GAO Lian¹; GU Da²

1. State Key Lab of High Performance Ceramics and Superfine Microstructure; Shanghai Institute of Ceramics; Chinese Academy of Sciences; Shanghai 20050; China; 2. Department of Chemistry of East China University of Science and Technology; Shanghai 200237; China

Received:2002-07-12 Revised:2002-10-30 Published:2003-07-20 Online:2003-07-20

Abstract

Abstract: ATO nanoparticles were prepared from Sn(OH)₄ nucleus grown uniformly with Sn(OH)4 and Sb(OH)₃ by a complex method. The effects of reaction conditions such as doping concentrations, pH, temperature and complexing agent/Sb on the resistance were investigated by means of TG-DTA,XRD,TEM. The results show that ATO nanoparticles synthesized possess tetrahedral rutile structure with an average grain size near 10nm and excellent electrical properties. TEM photographs show that the particles are weakly agglomerated.

Key words: ATO, nanoparticle, complex

CLC Number:

TB383

ZHANG Jian-Rong,GAO Lian,GU Da. Synthesis of Sb Doped Tin Oxide (ATO) Nanoparticles by Complex Method[J]. Journal of Inorganic Materials.

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Synthesis of Sb Doped Tin Oxide (ATO) Nanoparticles by Complex Method

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