无机材料学报

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Si3N4粉体表面分析及偶联剂作用量的选择

颜鲁婷; 司文捷; 苗赫濯; 齐龙浩   

  1. 清华大学材料系新型陶瓷与精细工艺国家重点实验室 北京 100084
  • 收稿日期:2001-09-17 修回日期:2001-11-06 出版日期:2002-09-20 网络出版日期:2002-09-20

Surface Chemistry Analysis of Si3N4 Powders and Selection of the Dosage of Coupling Agents

YAN Lu-Ting; SI Wen-Jie; MIAO He-Zhuo; QI Long-Hao   

  1. Department of Materials Science & Engineering; State Key Laboratory of New Ceramic and Fine Processing; Tsinghua University; Beijing 100084; China
  • Received:2001-09-17 Revised:2001-11-06 Published:2002-09-20 Online:2002-09-20

摘要: 在Si3N4粉体的生产和存储过程中,氧化和水解是两个不利的因素,但在偶联剂的作用下,它们在提高陶瓷粉体与有机载体的相容性方面起到了促进作用.本文测定了未经处理的Si3N4。粉及通过氧化和水解改性的Si3N4粉的表面性质,并分析了它们对偶联剂选择作用量的影响.

关键词: 表面分析, 氧化, 水解, 偶联剂

Abstract: Oxidation and hydrolization are disadvantageous factors in producing and storing Si3N4 powders. But it provides a convenience in the aspect improving the compatibility between inorganic ceramic powders and organic medium. In this article, the surface characters of as-received and modified powders were compared and their effect on the selection of coupling agents was also discussed.

Key words: surface analysis, oxidation, hydrolization, coupling agents

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