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无机材料学报

• 研究论文 • 上一篇    下一篇

定向SiC晶须增韧Si3N4陶瓷的制备及热震性能研究

罗学涛; 陈小君; 黄前军; 陈立富   

  1. 厦门大学材料科学与工程系 厦门 361005
  • 收稿日期:2003-05-23 修回日期:2003-09-08 出版日期:2004-05-20 网络出版日期:2004-05-20

Preparation and Thermal Shock Property of Si3N4 Ceramic Reinforced by Orientation SiC Whiskers

LUO Xue-Tao; CHEN Xian-Jun; HUANG Qian-Jun; CHEN Li-Fu   

  1. Department of Materials Science and Engineering; Xiamen University; Xiamen 361005; China
  • Received:2003-05-23 Revised:2003-09-08 Published:2004-05-20 Online:2004-05-20

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摘要： 通过SiC晶须在载体纤维中定向挤出和热压烧结工艺制备了高度定向SiC晶须增韧Si3N4复合材料,利用SEM观察了晶须的定向方向和复合材料的断口形貌. 实验结果表明,70％以上SiC晶须的定向角在0～10°之间,具有较好的方向性.过高的烧结温度和晶须含量使材料抗弯强度降低。晶须定向方向的断裂韧性(单迫切口垂直于定向晶须)比横向方向高出20％.1000和500℃温差的热震实验表明,定向SiC晶须复合材料比随机SiC晶须复合材料的抗热震性能高得多.

关键词: 氮化硅, 碳化硅晶须, 显微结构, 热震性能

Abstract: A highly orientation SiC whisker reinforced Si3N4 composite was fabricated by fiber extrusion and hot-pressing technique, which SiC whiskers were unidirectional oriented in the extruded carrier
fiber. Microstructure of the composites was observed by SEM. Whisker directions were image-processed to quantify SiC whisker orientation in the extruded fibers and the composites. Effects of sintering temperature
and SiC whisker content on the flexural strength and fracture toughness of the composites were investigated. The experimental results show that the flexural strength and fracture toughness of the orientation SiC whisker
toughened Si3N4 composites are higher than that of the random SiC whisker toughened Si3N4 composites after thermal shock experiment, in temperature difference of 1000℃ and 500℃.

Key words: Si3N4, SiC whiskers, microstructure, thermal shock property

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