Preparation of Nano TiN Powders and Influence Factors

Journal of Inorganic Materials

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Preparation of Nano TiN Powders and Influence Factors

LI Jing-Guo^1,2; GAO Lian¹; ZHANG Qing-Hong¹; SUN Jing¹; LI Wei¹

1.State Key Lab of High Performance Ceramics and Superfine Microstructure; Shanghai Institute of Ceramics; Chinese Academy of Sciences; Shanghai 200050; China; 2.Institute of Materials; Shandong University; Jinan 250061; China

Received:2002-05-13 Revised:2002-06-14 Published:2003-07-20 Online:2003-07-20

Abstract

Abstract: Nano TiN powders were prepared by the ammonium nitridation method using nano Ti0₂ powders as starting material. The effect of nitridation reaction conditions on the properties of nano TiN powders was studied. The purity of nano TiN powders was analyzed by the chemical method. The thermal stability of nano TiN powders was studied by the DTA-TG technique. The experimental results show that nitricled at 800℃for 5h, nano TiO₂ powders are completely converted into nano TiN powders. TEM micrographs show that the size of nano TiN particles is about 20nm.

Key words: nano TiN, nano TiO₂, preparation, influence factors

CLC Number:

TF123

LI Jing-Guo,GAO Lian,ZHANG Qing-Hong,SUN Jing,LI Wei. Preparation of Nano TiN Powders and Influence Factors[J]. Journal of Inorganic Materials.

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Preparation of Nano TiN Powders and Influence Factors

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