Journal of Inorganic Materials

• Research Paper • Previous Articles     Next Articles

Fabricating Transparent Yttria Ceramics at Low Temperature

WANG Jie-Qiang1; ZHENG Shao-Hua1; YUE Yun-Long1; TAO Zhen-Dong2; SUN Xu-Dong3   

  1. 1.Material School of Jinan University; Jinan 250022; China; 2.Material School of Shandong University; Jinan 250014, China; 3.Material and Metallurgy School of Northeastern University; Shenyang 110006; China
  • Received:2002-10-24 Revised:2002-12-16 Published:2003-11-20 Online:2003-11-20

Abstract: A new method for obtaining highly sinterable Y2O3 powders was developed. Those powders were used to prepare transparent bodies with
conventional sintering at relatively low temperature. Yttrium nitrate was used as a mother salt, and ammonia as a precipitant reagent, the fine
and dendritic precursor crystal was prepared by controlling the content of sulfate ions in the reaction system. The highly pure and low-agglomerated
Y2O3 powders were obtained by calcinating the precursor at 1100℃, the primary particles were spherical and about 60nm
in diameter. The powder compact pressed in steel die could be sintered to transparency without additives under vacuum at 1700℃. The sintered
transparent Y2O3 polycrystalline exhibited a homogeneous microstructure and its transmittance was up to 70% in the near infrared wavelength region.

Key words: low temperature, yttria, transparent ceramics, sulfate ion

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