Journal of Inorganic Materials

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Characterization of Microstructure and Properties of Post-hot Isostatic Pressing of Liquid Phase Sintered SiC

DONG Shaoming; CHEN Zhongming; TAN Shouhong; JIANG Dongliang; GUO Jingkun   

  1. Shanghai Institute of Ceratnics; Chinese Academy of Sciences Shanghai 200050 China
  • Received:1996-11-12 Revised:1997-01-13 Published:1997-12-20 Online:1997-12-20

Abstract: The microstructure and mechanical properties of liquid phase sintered SiC followed by post-hot isostatic pressing (HIP) were studied. It is indicated that the effect of post-HIP treatment is changed with the variation of
sintering aids and temperature of liquid phase sintering. After Ar-HIP treatment, the density of SiC is increased and the inside pores are
diminished, but grain growth is depressed. Besides the advantages of the Ar-HIP, N2-HIP can modify the surface state because of the reaction
between SiC and N2 so that the mechanical properties are improved. Microstructure analysis has shown that after N2-HIP treatment,
grain size is decreased and the density is increased. Meanwhile, the results of post-HIP treatment are highly affected by the microstructure
of the liquid phase sintered SiC. When the sintering temperature is relatively lower and the grain size is smaller, after post-HIP treatment, esp.
N2-HIP treatment, bending strength and fracture toughness of the liquid phase sintered SiC are improved greatly.

Key words: liquid phase sintering, SiC, post-hot isostatic pressing, microstructure, properties