Journal of Inorganic Materials

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2D SiC/SiC Manufactured by Chemical Vapor Infiltration: Narrow Band Random Vibration Fatigue Damage and Performance Degradation

LIU Mingyang1(), WANG Chun2, CHENG Pengfei2, MA Xuehan1, Gao Xiangyun3, YOU Bojie1, ZHAO Lufeng4, CHENG Laifei1,4, ZHANG Yi1,*()   

  1. 1 National Key Laboratory of Thermostructural Composite Materials, Northwestern Polytechnical University, Xi’an 710072, China
    2 AVIC Aircraft Strength Research Institute, Xi'an 710065, China
    3 Xi'an Aviation Brake Technology Co., Ltd, Xi'an 713106, China
    4 Xi'an Xinyao Ceramic Composite Material CO., LTD., Xi’an 710051, China

Abstract:

The operational requirements for high-temperature performance and structural weight reduction in aero-engine hot section components continue to intensify under demanding service conditions. Silicon carbide fiber reinforced silicon carbide matrix (SiC/SiC) composites are widely recognized as exceptionally promising alternative materials owing to their outstanding high-temperature stability, substantially reduced density, and superior corrosion resistance characteristics. However, under actual service enviroments, these composites inevitably experience complex vibrational loading spectra, with the consequent vibration induced fatigue damage accumulation emerging as a critical limiting factor in their practical engineering implementation. In this study, 2D SiC/SiC plates were fabricated by chemical vapor infiltration. Specimens featuring bilateral arc-shaped notches were machined from the plates and subsequently subjected to narrow band random vibration fatigue tests under the first order vibration mode. This experimental approach was undertaken specifically to investigate the progressive damage evolution process and the accompanying degradation patterns in tensile properties exhibited by the 2D SiC/SiC plate structure under vibrational fatigue loading. The research findings reveals that the normalized full time-domain characteristic curves of the 2D SiC/SiC plate structures exhibit progressive downward displacement as the applied equivalent stress amplitude (σe) increases. These curves concurrently manifest pronounced statistical dispersion throughout the low stress loading regime. Microstructural analyses enable the classification of the damage evolution within the 2D SiC/SiC plate structure into three distinct, sequential stages: the initial matrix damage stage, the subsequent interface damage stage, and the final fiber damage stage. Quantitatively, the damage progression rate follows a distinct three stage evolution—commencing with rapid progression, transitioning to reduced propagation velocity, and culminating in accelerated damage advancement during the terminal phase.The residual tensile properties demonstrate that the tensile characteristics of the 2D SiC/SiC plate structure follow an exponential decline trend. At a resonance frequency reduction of 31.9%, the tensile strength, proportional limit stress, elastic modulus, and resilience modulus have degraded to 270.0 MPa, 64.1 MPa, 106.3 GPa, and 0.020 MJ/m³, respectively — all falling below 70% of the corresponding values in the as-fabricated, pristine state. Subsequent analyses of the tensile fracture surface reveal matrix cracking and pronounced fiber wear as the dominant damage mechanisms responsible for the significant degradation observed in the tensile properties of the vibration fatigued composite structure. These findings provide critical experimental basis for assessing the service reliability of 2D SiC/SiC plate structures under vibrational service conditions.

Key words: 2D SiC/SiC, random vibration, fatigue damage, equivalent stress, tensile properties

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