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无机材料学报

• 研究论文 • 上一篇    下一篇

透明氮化铝陶瓷的制备

周艳平; 王岱峰; 奚益明; 庄汉锐; 温树林; 郭景坤; 严东生   

  1. 中国科学院上海硅酸盐研究所 上海 200050
  • 收稿日期:1998-09-14 修回日期:1998-10-16 出版日期:1999-08-20 网络出版日期:1999-08-20

Preparation of Translucent AlN Ceramics

ZHOU Yan-Ping, WANG Dai-Feng, XI Yi-Ming, ZHUANG Han-Rui, WEN Shu-Lin, GUO Jing-Kun, YAN Dong-Sheng   

  1. Shanghai Institute of Ceramics; Chinese Academy of Sciences Shanghai 200050 China
  • Received:1998-09-14 Revised:1998-10-16 Published:1999-08-20 Online:1999-08-20

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摘要： 本文采用碳热还原法制得的 Ａｌ Ｎ 粉， 使用烧结剂 Ｃａ Ｃ２ ， 热压制备了透明氮化铝陶瓷实验证明， 纯度高、粒径较小、且均匀的 Ａｌ Ｎ 粉是制备透明 Ａｌ Ｎ 陶瓷的必要条件 Ａｌ Ｎ 陶瓷从紫外、可见光到近红外均透明， 显微结构研究表明， Ａｌ Ｎ 陶瓷透明是由于晶粒完整规则， 紧密排列， 晶界干净， 而气孔、晶粒内和晶界第二相杂质、缺陷是影响透明度的原因.

关键词: 透明陶瓷, 氮化铝, 制备

Abstract: Translucent AlN ceramics were prepared by hot pressing with AlN powder synthesized by using carbon thermal reducing method and additive CaC2. The experiments
show that the AlN powder with high purity, small particle size and narrow size distribution is necessary for translucent AlN ceramics. CaC2 is an effective sintering
additive for translucent AlN ceramics, improving the densification of AlN and evaporating cleaning the grain boundary. The product is translucent in the range
of ultraviolet to infrared. The microstructure study shows that the translucent reason is the grains of AlN complete growing and closely arranging.

Key words: translucent ceramic，aluminum nitride，preparation

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