Preparation and Characterization of Layered Compound of Na3Sb3P2O14

Journal of Inorganic Materials

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Preparation and Characterization of Layered Compound of Na₃Sb₃P₂O₁₄

YANG Gang; LONG Xiang-Yun

School of Chemistry and Chemical Engineering; Guangxi University; Nanning 530004; China

Received:2000-01-07 Revised:2000-02-25 Published:2001-05-20 Online:2001-05-20

Abstract

Abstract: A new compound, NA₃Sb₃P₂O₁₄, was first synthesized by microwave and conventional synthetic methods. The same product can be obtained from two kinds of reacting substances and in different reaction conditions. The material was characterized by XRD, IR, SEM and characterization program. The compound is tetragonal with a=3.6424(5)A, c=5.9488A, and has a layered structure with an interlayer space of 5.95A.

Key words: layer compound, sodium phosphatoantimonate, synthesis, characterization

CLC Number:

TB34

YANG Gang,LONG Xiang-Yun. Preparation and Characterization of Layered Compound of Na₃Sb₃P₂O₁₄[J]. Journal of Inorganic Materials.

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Preparation and Characterization of Layered Compound of Na₃Sb₃P₂O₁₄

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