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无机材料学报

无机材料学报

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锆钛酸铅95/5纳米粉体Sol-Gel法制备与改进

谢湘华1; 董亚明1; 姚春华2; 瞿翠凤2; 董显林2   

  1. 1. 华东理工大学, 上海 200237; 2. 中国科学院上海硅酸盐研究所, 上海 200050
  • 收稿日期:2002-12-30 修回日期:2003-02-19 出版日期:2004-01-20 网络出版日期:2004-01-20

Preparation of PZT95/5 Nano-powders with Modified Sol-Gel Method

XIE Xiang-Hua1; DONG Ya-Ming1; YAO Chun-Hua2; QU Cui-Feng2; DONG Xian-Lin2   

  1. 1.East China University of Science and Technology; Shanghai 200237 China; 2. Shanghai Institute of Ceramics Chinese Academy of Sciences; Shanghai 200050; China
  • Received:2002-12-30 Revised:2003-02-19 Published:2004-01-20 Online:2004-01-20

PDF (PC)

1116

被引次数

30

摘要： 以醋酸铅、硝酸锆、钛酸丁酯为原料,改进溶胶-凝胶法,制备得到锆钛酸铅95/5纳米粉体.改进溶胶-凝胶法省去溶胶加水、凝胶干燥、干凝胶研磨等步骤,采用加热蒸馏溶胶制备凝胶,蒸馏回收溶剂并干燥凝胶,凝胶分段加热处理等方法,简化了加工工艺,大大缩短了合成周期,降低了成本.XRD和TEM分析表明,用改进sol-gel法制备得到的PZT粉体煅烧温度低、晶粒细小、均匀,直径约10nm.

关键词: PZT, sol-gel, 纳米, 合成

Abstract: PbZr0.95Ti0.05O3 nano-powders were synthesized with a modified sol-gel method at low calcining temperatures. Pb(CH3COO)2·3H2O, Zr(NO3)4·5H2O and Ti(C4H9O)4 were used as parent reagents. The sol-gel method was modified by cutting down certain procedures and calcining wet gel in a proper heating sequence. XRD and TEM testy show that the PZT nano-particles are ultrafine and uniform, their diameters are around 10 nanometers.

Key words: PZT, sol-gel, nano-powders, synthesize

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