Journal of Inorganic Materials ›› 2012, Vol. 27 ›› Issue (4): 343-347.DOI: 10.3724/SP.J.1077.2012.00343
• Orginal Article • Previous Articles Next Articles
YAO Xiu-Qiong, HE Jie-Yu, YANG Jin, HOU Shan-Hua, OUYANG Jian-Ming
Received:
2011-04-29
Revised:
2011-09-05
Published:
2012-04-10
Online:
2012-03-12
About author:
YAO Xiu-Qiong. E-mail: yaoxiuqiong-2006@163.com
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CLC Number:
YAO Xiu-Qiong, HE Jie-Yu, YANG Jin, HOU Shan-Hua, OUYANG Jian-Ming. Aggregation of Urinary Microcrystallines with Different Sizes[J]. Journal of Inorganic Materials, 2012, 27(4): 343-347.
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Membrane pore size /μm | Placing time, t / h | Δ | |||||
---|---|---|---|---|---|---|---|
0 | 0.5 | 1 | 2 | 4 | |||
0.22 | 167±80 | 533±144 | 854±193 | 1041±211 | 1606±281 | 1439 | |
Stone formers | 0.45 | 295±115 | 731±170 | 1124±224 | 1386±335 | 1852±373 | 1557 |
1.2 | 772±210 | 1392±311 | 1831±310 | 1910±296 | 2306±379 | 1534 | |
3 | 1718±355 | 2060±259 | 2337±331 | 2509±390 | 2769±394 | 1051 | |
10 | 3251±531 | 2267±642 | 1657±261 | 3140±279 | 1550±352 | ? | |
0.22 | 194±69 | 324±123 | 499±198 | 423±141 | 668±228 | 474 | |
Healthy subjects | 0.45 | 375±132 | 503±181 | 596±149 | 689±167 | 886±193 | 511 |
1.2 | 457±143 | 619±156 | 690±201 | 806±194 | 1024±218 | 567 | |
3 | 615±213 | 655±187 | 731±146 | 921±215 | 1048±282 | 433 | |
10 | 721±231 | 751±251 | 838±213 | 959±311 | 1100±267 | 379 |
Table 1 Change of average size of urinary crystallites filtrated by microporous membrane with different pore sizes and different placing time / nm
Membrane pore size /μm | Placing time, t / h | Δ | |||||
---|---|---|---|---|---|---|---|
0 | 0.5 | 1 | 2 | 4 | |||
0.22 | 167±80 | 533±144 | 854±193 | 1041±211 | 1606±281 | 1439 | |
Stone formers | 0.45 | 295±115 | 731±170 | 1124±224 | 1386±335 | 1852±373 | 1557 |
1.2 | 772±210 | 1392±311 | 1831±310 | 1910±296 | 2306±379 | 1534 | |
3 | 1718±355 | 2060±259 | 2337±331 | 2509±390 | 2769±394 | 1051 | |
10 | 3251±531 | 2267±642 | 1657±261 | 3140±279 | 1550±352 | ? | |
0.22 | 194±69 | 324±123 | 499±198 | 423±141 | 668±228 | 474 | |
Healthy subjects | 0.45 | 375±132 | 503±181 | 596±149 | 689±167 | 886±193 | 511 |
1.2 | 457±143 | 619±156 | 690±201 | 806±194 | 1024±218 | 567 | |
3 | 615±213 | 655±187 | 731±146 | 921±215 | 1048±282 | 433 | |
10 | 721±231 | 751±251 | 838±213 | 959±311 | 1100±267 | 379 |
Fig. 2 TEM images of urinary crystallites of CaOxa stone former (a) and healthy subject (b) filtrated by 0.45 mm pore membrane after placing for different time
Instruments / μm | Placement time / h | |||||
---|---|---|---|---|---|---|
0 | 0.5 | 1 | 2 | 4 | ||
Stone former | NSA results / nm | 295±115 | 731±170 | 1124±224 | 1386±335 | 1852±373 |
TEM results / nm | 275 | 1050 | 1600 | |||
Healthy subject | NSA results / nm | 375±132 | 503±181 | 596±149 | 689±167 | 886±193 |
TEM results / nm | 170 | 300 | 600 |
Table 2 Comparison of urinary crystallites size determined by TEM and nanoparticle size analyzer respectively after filtrated by 0.45 mm pore membrane / nm
Instruments / μm | Placement time / h | |||||
---|---|---|---|---|---|---|
0 | 0.5 | 1 | 2 | 4 | ||
Stone former | NSA results / nm | 295±115 | 731±170 | 1124±224 | 1386±335 | 1852±373 |
TEM results / nm | 275 | 1050 | 1600 | |||
Healthy subject | NSA results / nm | 375±132 | 503±181 | 596±149 | 689±167 | 886±193 |
TEM results / nm | 170 | 300 | 600 |
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