Journal of Inorganic Materials ›› 2011, Vol. 26 ›› Issue (10): 1085-1089.DOI: 10.3724/SP.J.1077.2011.01085

• Research Paper • Previous Articles     Next Articles

Synthesis of Amphiphilic Silica Nanocomposites

JIA Zhong-Qi, LI Xiao-Xuan, XIAO Zheng-Hui, WANG Wen-Ping, CAO Nan-Nan   

  1. (School of Chemical and Engineering, Hefei University of Technology, Hefei 230009, China)
  • Received:2010-12-09 Revised:2011-03-08 Published:2011-10-20 Online:2011-09-20
  • Supported by:

    National Natural Science Foundation of China (50673023)

Abstract: Silica modified by γ-glycidyloxypropyltrimethoxysilane was used as precursor to prepare amphiphilic silica nanocomposites by quaterisation. The structure of the as-prepared products was characterized by means of fourier transform infrared (FTIR), thermogravimetric analysis (TGA) and X-ray photoelectron spectroscope (XPS). Transmission electron microscopie (TEM) was used to characterize the morphology of the nanocomposites. The results showed that the content of the organic components at the silica surface calculated from TGA data was 11wt%. TEM provided direct evidence for the well amphiphilicity, and the same conclusion was confirmed by the photographs of the pristine SiO2 and surface-modified SiO2 nanocomposites in water/toluene mixed layers.

Key words: nano-SiO2, surface modification, nanocomposites, amphiphilicity

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