Synthesis of Yttria-Stabilized Zirconia Nanoparticles by Heating of Alcohol-Aqueous Salt Solutions

Abstract

Abstract: A novel method which involved the heating of a ZrOCl₂ and Y(NO₃)₃ solution with an alcohol-water mixture as a solvent was used to synthesize the
nanoparticles of ZrO₂(3Y). By choosing the composition of the solvent mixture and adding appropriate dispersant, weakly agglomerated powders of ZrO₂(3Y)
with the average particle size of 11～15nm can be obtained. Contrast with the ordinary trend of the powder synthesized by coprecipitation, the monoclinic
phase in this powder decreases when the calcination temperature rising from 600℃ to 900℃, the mechanism of this phenomenon was investigated.
High-density and fine-particle Y-TZP ceramics were obtained by pressureless sintering.

Key words: heating of alcohol-aqueous salt solutions, ZrO₂(3Y), nanoparticles

CLC Number:

TF123

LI Wei,GAO Lian,GUO Jing-Kun. Synthesis of Yttria-Stabilized Zirconia Nanoparticles by Heating of Alcohol-Aqueous Salt Solutions[J]. Journal of Inorganic Materials.

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Synthesis of Yttria-Stabilized Zirconia Nanoparticles by Heating of Alcohol-Aqueous Salt Solutions

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