Preparation of Nanocrystal TiO2 with Rutile Structure at Lower Temperature from TiOCl2 Solution

Abstract

Abstract: Nanometer titania needle-shaped agglomeration was directly prepared by aging TiOCl₂ aqueous solution from room temperature to 60°C. The effect of reaction temperature and stirring on TiO₂ crystalline size and morphology were discussed. The results show the morphology of product is pseudo-sphere in the stirring condition. The aging temperatures have no effect on the morphology of product. The TiO₂ particles were characterized by TEM and XRD. The result shows the product is nanometer titania needle-shaped agglomeration with rutile structure.

Key words: titania, nanoparticles, rutile

CLC Number:

TF123

ZHANG Yan-Feng,WEI Yu,JIA Zhen-Bin,HAN Mei-Juan,WANG Ping. Preparation of Nanocrystal TiO₂ with Rutile Structure at Lower Temperature from TiOCl₂ Solution[J]. Journal of Inorganic Materials.

[1]	YU Man, GAO Rongyao, QIN Yujun, AI Xicheng. Influence of Upconversion Luminescent Nanoparticles on Hysteresis Effect and Ion Migration Kinetics in Perovskite Solar Cells [J]. Journal of Inorganic Materials, 2024, 39(4): 359-366.
[2]	YU Yefan, XU Ling, NI Zhongbing, SHI Dongjian, CHEN Mingqing. Prussian Blue Modified Biochar: Preparation and Adsorption of Ammonia Nitrogen from Sewage [J]. Journal of Inorganic Materials, 2023, 38(2): 205-212.
[3]	WANG Mengtao, SUO Jun, FANG Dong, YI Jianhong, LIU Yichun, Olim RUZIMURADOV. Visible-light Catalytic Performance of ITO/TiO₂ Nanotube Array Composite [J]. Journal of Inorganic Materials, 2023, 38(11): 1292-1300.
[4]	WANG Xiaojun, XU Wen, LIU Runlu, PAN Hui, ZHU Shenmin. Preparation and Properties of Ag@C₃N₄ Photocatalyst Supported by Hydrogel [J]. Journal of Inorganic Materials, 2022, 37(7): 731-740.
[5]	MA Hui, TAO Jianghui, WANG Yanni, HAN Yu, WANG Yabin, DING Xiuping. Gold Nanoparticles Supported on Silica & Titania Hybrid Mesoporous Spheres and Their Catalytic Performance Regulation [J]. Journal of Inorganic Materials, 2022, 37(4): 404-412.
[6]	SU Li, YANG Jianping, LAN Yue, WANG Lianjun, JIANG Wan. Interface Design of Iron Nanoparticles for Environmental Remediation [J]. Journal of Inorganic Materials, 2021, 36(6): 561-569.
[7]	ZHANG Yiqing,ZHANG Shujuan,WAN Zhengrui,MO Han,WANG Niangui,ZHOU Liqun. RuFe Nanoparticles Modified Sheet-like BiVO₄ : High-efficient Synergistic Catalyst for Ammonia Borane Hydrolytic Dehydrogenation [J]. Journal of Inorganic Materials, 2020, 35(7): 809-816.
[8]	SHAO Kang,WANG Tao,WEN Yingting,TENG Yuanjie,LIU Huijun,PAN Zaifa. Modulation of Morphology and Luminescence Property of NaBiF₄:Yb³⁺/Er³⁺ Upconversion Nanoparticles by Organic Ligands [J]. Journal of Inorganic Materials, 2020, 35(4): 447-453.
[9]	GUO Si-Lin, KANG Shuai, LU Wen-Qiang. Ge Nanoparticles in MXene Sheets: One-step Synthesis and Highly Improved Electrochemical Property in Lithium-ion Batteries [J]. Journal of Inorganic Materials, 2020, 35(1): 105-111.
[10]	LI Sheng-Song, ZHENG Yong-Chao, MENG Shu-Lin, WU Li-Zhu, ZHONG Jin- Yi, ZHAO Chong-Lin. Core/Shell Quantum Dots and Au Nanoparticles Assembly for Effective Detection of Nerve Agent Mimic [J]. Journal of Inorganic Materials, 2019, 34(8): 893-898.
[11]	ZHU Meng-Meng, LI Guo-Hua, ZHANG Xue-Ming, ZHAI Jia-Xin, GAN Si-Ping, SONG Xiao. Boron Nitride Nanosheets Supported Cu₂O Nanoparticles: Synthesis and Catalytic Reduction for 4-nitrophenol [J]. Journal of Inorganic Materials, 2019, 34(8): 817-826.
[12]	CHENG Tian-Sheng, PAN Jiong, XU Ying-Ying, BAO Qun-Qun, HU Ping, SHI Jian-Lin. Synthesis of Zn, Mn doped Fe₃O₄ Nanoparticles with Tunable Size [J]. Journal of Inorganic Materials, 2019, 34(8): 899-903.
[13]	WANG Ya, SUO Hong-Li, LIU Min, WANG Tian-Tian, KAUSAR Shaheen, XU Yan, MA Lin. Property of YBCO Films Doping with Positive and Negative Lattice Mismatch Nanoparticles [J]. Journal of Inorganic Materials, 2019, 34(8): 857-861.
[14]	WANG Ya, SUO Hong-Li, MAO Lei, LIU Min, MA Lin, WANG Yi, KAUSAR Shaheen, ZHOU Yu-Qi. Flux Pinning Mechanism of Nb-doped YBCO Film [J]. Journal of Inorganic Materials, 2019, 34(10): 1055-1059.
[15]	SHENG Peng, ZHAO Guang-Yao, XU Li, LIU Shuang-Yu, WANG Bo, LIU Hai-Zhen, MA Guang, HAN Yu, CHEN Xin. Reductive Preparation of Blue TiO₂ via Deposition of Aluminum [J]. Journal of Inorganic Materials, 2018, 33(9): 942-948.

Preparation of Nanocrystal TiO₂ with Rutile Structure at Lower Temperature from TiOCl₂ Solution

PDF (PC)

Knowledge

Abstract

Cite this article

share this article

References

Related Articles 15

Recommended Articles

Metrics

Comments