Preparation of Monodispersed Nanometer Titanium Dioxide by the Complex from Titanium Tetrachloride

Abstract

Abstract: Monodispersed titanium dioxide nanoparticles were prepared by the hydrolysis of the titanium complex at 145℃ , the complex was obtained by the reaction of TiCl₄, with tri- ethanolamine. The crystalline phase and morphology of the nanoparticles were characterized by means of TEM and XRD techniques. The sizes of the particles can be regulated by changing pH values of the complex solution. The UV spectra of the complex solution were measured. The formation and hydrolysis of the complex were discussed.

Key words: titanium dioxide, nanoparticle, monodispersion, anatase

CLC Number:

TF123

CHEN Hong-Ling,WANG Yan-Ru,SHI Jun. Preparation of Monodispersed Nanometer Titanium Dioxide by the Complex from Titanium Tetrachloride[J]. Journal of Inorganic Materials.

[1]	MA Binbin, ZHONG Wanling, HAN Jian, CHEN Liangyu, SUN Jingjing, LEI Caixia. ZIF-8/TiO₂ Composite Mesocrystals: Preparation and Photocatalytic Activity [J]. Journal of Inorganic Materials, 2024, 39(8): 937-944.
[2]	CAI Heqing, HAN Lu, YANG Songsong, XUE Xinyu, ZHANG Kou, SUN Zhicheng, LIU Ruping, HU Kun, WEI Yan. Fe₃O₄-DMSA-PEI Magnetic Nanoparticles with Small Particle Size: Preparation and Gene Loading [J]. Journal of Inorganic Materials, 2024, 39(5): 517-524.
[3]	YU Man, GAO Rongyao, QIN Yujun, AI Xicheng. Influence of Upconversion Luminescent Nanoparticles on Hysteresis Effect and Ion Migration Kinetics in Perovskite Solar Cells [J]. Journal of Inorganic Materials, 2024, 39(4): 359-366.
[4]	WANG Zhaoyang, QIN Peng, JIANG Yin, FENG Xiaobo, YANG Peizhi, HUANG Fuqiang. Sandwich Structured Ru@TiO₂ Composite for Efficient Photocatalytic Tetracycline Degradation [J]. Journal of Inorganic Materials, 2024, 39(4): 383-389.
[5]	WANG Shiyi, FENG Aihu, LI Xiaoyan, YU Yun. Pb (II) Adsorption Process of Fe₃O₄ Supported Ti₃C₂T_x [J]. Journal of Inorganic Materials, 2023, 38(5): 521-528.
[6]	YU Yefan, XU Ling, NI Zhongbing, SHI Dongjian, CHEN Mingqing. Prussian Blue Modified Biochar: Preparation and Adsorption of Ammonia Nitrogen from Sewage [J]. Journal of Inorganic Materials, 2023, 38(2): 205-212.
[7]	XUE Hongyun, WANG Congyu, MAHMOOD Asad, YU Jiajun, WANG Yan, XIE Xiaofeng, SUN Jing. Two-dimensional g-C₃N₄ Compositing with Ag-TiO₂ as Deactivation Resistant Photocatalyst for Degradation of Gaseous Acetaldehyde [J]. Journal of Inorganic Materials, 2022, 37(8): 865-872.
[8]	CHI Congcong, QU Panpan, REN Chaonan, XU Xin, BAI Feifei, ZHANG Danjie. Preparation of SiO₂@Ag@SiO₂@TiO₂ Core-shell Structure and Its Photocatalytic Degradation Property [J]. Journal of Inorganic Materials, 2022, 37(7): 750-756.
[9]	WANG Xiaojun, XU Wen, LIU Runlu, PAN Hui, ZHU Shenmin. Preparation and Properties of Ag@C₃N₄ Photocatalyst Supported by Hydrogel [J]. Journal of Inorganic Materials, 2022, 37(7): 731-740.
[10]	MA Hui, TAO Jianghui, WANG Yanni, HAN Yu, WANG Yabin, DING Xiuping. Gold Nanoparticles Supported on Silica & Titania Hybrid Mesoporous Spheres and Their Catalytic Performance Regulation [J]. Journal of Inorganic Materials, 2022, 37(4): 404-412.
[11]	CAI Jia, HUANG Gaoxu, JIN Xiaopan, WEI Chi, MAO Jiayi, LI Yongsheng. In-situ Modification of Carbon Nanotubes with Metallic Bismuth Nanoparticles for Uniform Lithium Deposition [J]. Journal of Inorganic Materials, 2022, 37(12): 1337-1343.
[12]	SU Li, YANG Jianping, LAN Yue, WANG Lianjun, JIANG Wan. Interface Design of Iron Nanoparticles for Environmental Remediation [J]. Journal of Inorganic Materials, 2021, 36(6): 561-569.
[13]	XI Wen, LI Haibo. Preparation of TiO₂/Ti₃C₂T_x Composite for Hybrid Capacitive Deionization [J]. Journal of Inorganic Materials, 2021, 36(3): 283-291.
[14]	JIN Gaoyao, HE Haichuan, WU Jie, ZHANG Mengyuan, LI Yajuan, LIU Younian. Cobalt-doped Hollow Carbon Framework as Sulfur Host for the Cathode of Lithium Sulfur Battery [J]. Journal of Inorganic Materials, 2021, 36(2): 203-209.
[15]	PAN Bichen,REN Penghe,ZHOU Tejun,CAI Zhenyang,ZHAO Xiaojun,ZHOU Hongming,XIAO Lairong. Microstructure and Property of Thermal Insulation Coating on the Carbon Fiber Reinforced Epoxy Resin Composites [J]. Journal of Inorganic Materials, 2020, 35(8): 947-952.

Preparation of Monodispersed Nanometer Titanium Dioxide by the Complex from Titanium Tetrachloride

PDF (PC)

Knowledge

Cited

Abstract

Cite this article

share this article

References

Related Articles 15

Recommended Articles

Metrics

Comments