陈化过程中湿度、温度及时间对Nd:YAG纳米粉体的影响

doi:10.3724/SP.J.1077.2011.01273

无机材料学报 ›› 2011, Vol. 26 ›› Issue (12): 1273-1280.DOI: 10.3724/SP.J.1077.2011.01273 CSTR: 32189.14.SP.J.1077.2011.01273

陈化过程中湿度、温度及时间对Nd:YAG纳米粉体的影响

张晓琳, 刘铎, 秦海明, 刘宏, 王继扬, 桑元华

(山东大学晶体材料国家重点实验室, 济南 250010)

收稿日期:2011-01-04 修回日期:2011-03-25 出版日期:2011-12-20 网络出版日期:2011-11-11
作者简介:张晓琳(1981-), 女, 博士研究生. E-mail: zxl_sd@yahoo.cn
基金资助:
国家自然科学基金(50702031, 60974117, 50990303); 973项目(2009CB30503, G2004CB619002)

Effects of Humidity, Temperature and Time on the Nd:YAG Nano-powders during the Aging Process

ZHANG Xiao-Lin, LIU Duo, QIN Hai-Ming, LIU Hong, WANG Ji-Yang, SANG Yuan-Hua

(State Key Laboratory of Crystal Materials, Shandong University, Jinan 250100, China)

Received:2011-01-04 Revised:2011-03-25 Published:2011-12-20 Online:2011-11-11
About author:ZHANG Xiao-Lin. E-mail: zxl_sd@yahoo.cn
Supported by:
National Natural Science Foundation of China (50702031, 60974117, 50990303); 973 Program of China (2009CB30503, G2004CB619002)

摘要/Abstract

摘要： 采用微波辅助均相沉淀法制备了Nd:YAG(Nd:Y₃Al₅O₁₂)纳米粉体. 通过XRD和SEM对此方法制备的Nd:YAG纳米粉体进行了分析表征, 并分析了在陈化过程中, 湿度、温度和陈化时间对制备Nd:YAG纳米粉体的影响. 实验结果表明: 陈化环境的湿度、温度和陈化时间对制备Nd:YAG纳米粉体的组分和形貌有显著的影响. 陈化环境中湿度和温度对Nd:YAG纳米粉体的影响具有一定的依存关系, 必须适当地控制; 陈化时间对Nd:YAG纳米粉体的粒径大小影响显著, 随着陈化时间的延长, 获得的Nd:YAG纳米粉体的颗粒尺寸先减小后增大.

关键词: Nd:YAG, 纳米粉体, 湿度, 陈化

Abstract: The Nd:YAG (Nd:Y₃Al₅O₁₂) nano-powders were successfully prepared by the microwave-assisted homogeneous precipitation method. The Nd:YAG nano-powders were analyzed by means of XRD and SEM. The effects of humidity, temperature and aging time during the aging process on the preparation of the Nd:YAG nano-powders were discussed. The results show that the composition and morphology of the Nd:YAG precursors and Nd:YAG nano-powders are remarkably affected by the above factors. Effects of environmental humidity and temperature on the preparation of the Nd:YAG nano-powders are dependent on each other, which must be properly controlled. And the aging time can significantly affect sizes of the Nd:YAG nano-powders. Particle size of the Nd:YAG nano-powder decreases and then increases with the aging time increasing.

Key words: Nd:YAG, nano-powders, humidity, aging

中图分类号:

TB32

张晓琳, 刘铎, 秦海明, 刘宏, 王继扬, 桑元华. 陈化过程中湿度、温度及时间对Nd:YAG纳米粉体的影响[J]. 无机材料学报, 2011, 26(12): 1273-1280.

ZHANG Xiao-Lin, LIU Duo, QIN Hai-Ming, LIU Hong, WANG Ji-Yang, SANG Yuan-Hua. Effects of Humidity, Temperature and Time on the Nd:YAG Nano-powders during the Aging Process[J]. Journal of Inorganic Materials, 2011, 26(12): 1273-1280.

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陈化过程中湿度、温度及时间对Nd:YAG纳米粉体的影响

Effects of Humidity, Temperature and Time on the Nd:YAG Nano-powders during the Aging Process

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