C/SiC复合材料有序多孔陶瓷接头的制备及其连接技术研究

doi:10.3724/SP.J.1077.2013.12556

无机材料学报 ›› 2013, Vol. 28 ›› Issue (7): 763-768.DOI: 10.3724/SP.J.1077.2013.12556 CSTR: 32189.14.SP.J.1077.2013.12556

C/SiC复合材料有序多孔陶瓷接头的制备及其连接技术研究

王浩, 周卿军, 简科, 邵长伟, 朱旖华

(国防科学技术大学新型陶瓷纤维及其复合材料重点实验室, 长沙 410073)

收稿日期:2012-09-13 修回日期:2012-12-01 出版日期:2013-07-20 网络出版日期:2013-06-19
基金资助:
国家自然科学基金(50702075, 51172280); 湖南省杰出青年基金(12JJ1008); 湖南省高校科技创新团队支持计划(2012)

Preparation of Ordered Porous Ceramic Joint on C/SiC Composites and Its Joining Technique

WANG Hao, ZHOU Qing-Jun, JIAN Ke, SHAO Chang-Wei, ZHU Yi-Hua

(Science and Technology on Advanced Ceramic Fibers and Composites Laboratory, National University of Defense Technology, Changsha 410073, China)

Received:2012-09-13 Revised:2012-12-01 Published:2013-07-20 Online:2013-06-19
Supported by:
National Natural Science Foundation of China (50702075, 51172280); Hunan Provincial Science Fund for Distinguished Young Scholars (12JJ1008); Aid Program for Science and Technology Innovative Research Team in Higher Educational Institutions of Hunan Province (2012)

摘要/Abstract

摘要： 采用stöber法制备出单分散氧化硅小球, 并以此为模板, 结合先驱体转化技术成功制备出C/SiC复合材料纳米有序多孔陶瓷接头, 并对该接头制备工艺条件作了优化。对制备出的C/SiC多孔陶瓷接头分别采用先连后浸法(SJM)和直接浸渍法(DSM)进行了连接。结果显示, 两种方法连接的连接件的抗弯强度分别达82.4和20.5 MPa, 表明C/SiC多孔陶瓷接头采用SJM连接较好。

关键词: C/SiC复合材料, 连接, 先驱体转化技术, 模板技术, 有序多孔陶瓷接头

Abstract: Mono-dispersed silica spheres were prepared as template by st?ber method. Based on this template, the ordered nanoporous ceramic joints on the C/SiC composites were successfully fabricated for the first time by preceramic polymer techniques and the condition was optimized. Two different joining methods, directly soaking (DSM) and soaking after the first joining (SJM), were used for joining the ordered nanoporous ceramic joints of the C/SiC composites. The result shows that the bending strength of the joints by DSM and SJM is about 20.5 and 82.4 MPa, respectively, suggesting SJM more suitable for joining C/SiC composites.

Key words: C/SiC composites, joining, precursor conversion technique, template technique, ordered nanoporous ceramic joint

中图分类号:

TQ174

王浩, 周卿军, 简科, 邵长伟, 朱旖华. C/SiC复合材料有序多孔陶瓷接头的制备及其连接技术研究[J]. 无机材料学报, 2013, 28(7): 763-768.

WANG Hao, ZHOU Qing-Jun, JIAN Ke, SHAO Chang-Wei, ZHU Yi-Hua. Preparation of Ordered Porous Ceramic Joint on C/SiC Composites and Its Joining Technique[J]. Journal of Inorganic Materials, 2013, 28(7): 763-768.

参考文献

[1] Sanokawa Y, Ido Y, Sohda Y, et al. Application of continuous fiber reinforced silicon carbide matrix composites to a ceramic gas turbine model for automobile. Ceram. Eng. & Sc. Proc., 1997, 18(4): 221–228.

[2] Wulz H G, Trabandt U. Large integral hot CMC structures designed for future reusable launchers. AIAA-97-2485.

[3] Murata H, Shioda M, Nakamura T. Method and Apparatus for Manufacturing Ceramic-based Composite Member. United States, B28B13/00, US 6, 723, 381. 2004.

[4] Yamaguchi H, Nakamura T, Murata H. Method for Fabricating Ceramic Matrix Composite. United States, C04B 35/80, US 6, 723, 382. 2004.

[5] Schmidt S, Beyer S, Knabe H, et al. Advanced Ceramic Matrix Composites Materials for Current and Future Propulsion Technology Applications. IAC-03-S.3, Germany, 03 Sep, 2003.

[6] Velev O D, Jede T A, Lobo R F, et al. Porous silica via colloidal crystallization. Nature, 1997, 389: 447–448.

[7] Velev O D, Jede T A, Lobo R F, et al. Microstructured porous silica obtained via colloidal crystal templates. Chem. Mater., 1998, 10(11): 3597–3602.

[8] Stein A, Schroden R C. Colloidal crystal templating of three-dimensionally ordered macroporous solids: materials for photonics and beyond. Current Opinion in Solid State & Materials Science, 2001, 5(6): 553-564.

[9] Yan H, Blanford C F, Holland B T, et al. General synthesis of periodic macroporous solids by templated salt precipitation and chemical conversion. Chem. Mater., 2000, 12(4): 1134–1141.

[10] Yu J S, Yoon S B, Chai G S. Ordered uniform porous carbon by carbonization of sugars. Carbon, 2001, 39: 1421–1425.

[11] Bartlett P N, Birkin P R, Ghanem M A, et al. Electrochemical syntheses of highly ordered macroporous conducting polymers grown around self-assembled colloidal templates. J. Mater. Chem., 2001, 11(3): 849–853.

[12] Yi D K, Kim D Y. Novel approach to the fabrication of macroporous polymers and their use as a template for crystalline titania nanorings. Nano Lett., 2003, 3(2): 207–211.

[13] Beck J S, Vartuli J C, Roth W J. A new family of mesoporous molecular sieves prepared with liquid crystal templates. J. Am. Chem. Soc., 1992, 114(24): 10834-10843.

[14] Wang H, Zheng S Y, Li X D, et al. Preparation of three-dimensional ordered macroporous SiCN ceramic using sacrificing template method. Microporous and Mesoporous Mater., 2005, 80(1/2/3): 357-362.

[15] Chen C Y, Xiao S Q, Davis M E. Studies on ordered mesoporous materials III. Comparison of MCM-41 to mesoporous materials derived from kanemite. Microporous Mater., 1995, 4(1): 1-20.

[16] Yanagisawa T, Shimizu T, Kuroda K, et al. The preparation of alkyltrimethylammoniumkanemite complexes and their conversion tomicroporous materials. Bull. Chem. Soc. Jpn., 1990, 63(4): 988-992.

[17] Huo Q, Leon R, Petroff P M, et al. Mesostructure design with gemini surfactants: supercage formation in a 3-D hexagonal array. Science, 1995, 268(5215): 1324-1327.

[18] Sakamoto Y, Kaneda M, Teraski O, et al. Direct imaging of the pores and cages of three-dimensional mesoporous materials. Nature, 2000, 408(6811): 449-453.

[19] Wang H, Li X D, Yu J S , et al. Fabrication and characterization of ordered macroporous PMS-derived SiC from a sacrificial template method. J. Mater. Chem., 2004, 14: 1383-1386.

[20] St?ber W, Fink A, Bohn E. Controlled growth of monodispersed silica spheres in the micron size range. J. Colloid. Interface Sci., 1968, 26(1): 62-69.

[21] Areán C O, Delgado M R, Montouillout V, et al. NMR and FTIR spectroscopic studies on the acidity of gallia-silica prepared by a Sol-Gel route. Microporous and Mesoporous Mater., 2004, 67(2/3): 259-264.

[22] 所俊. SiC陶瓷及其复合材料的先驱体高温连接及陶瓷金属梯度材料的制备与连接研究. 长沙: 国防科学技术大学博士论文, 2005.

[23] LUO Zhao-Hua, JIANG Dong-Liang, ZHANG Jing-Xian, et al. Thermal shock behavior of the SiC-SiC joints joined with Na2O-B2O3-SiO2 glass solder. Journal of Inorganic Materials, 2012, 27(3): 234-238.

C/SiC复合材料有序多孔陶瓷接头的制备及其连接技术研究

Preparation of Ordered Porous Ceramic Joint on C/SiC Composites and Its Joining Technique

RichHTML

PDF (PC)

可视化

被引次数

摘要/Abstract

引用本文

使用本文

参考文献

相关文章 15

编辑推荐

Metrics

本文评价

[1]	全文心, 余艺平, 方冰, 李伟, 王松. 管状C/SiC复合材料高温空气氧化行为与宏细观建模研究[J]. 无机材料学报, 2024, 39(8): 920-928.
[2]	王润, 相恒阳, 曾海波. 钙钛矿多色级联发光二极管中多中心载流子均衡分布调控研究[J]. 无机材料学报, 2023, 38(9): 1062-1068.
[3]	刘岩, 张珂颖, 李天宇, 周菠, 刘学建, 黄政仁. 陶瓷材料电场辅助连接技术研究现状及发展趋势[J]. 无机材料学报, 2023, 38(2): 113-124.
[4]	刘金铃, 刘佃光, 任科, 王一光. 氧化物陶瓷闪烧机理及其应用研究进展[J]. 无机材料学报, 2022, 37(5): 473-480.
[5]	王洪达, 冯倩, 游潇, 周海军, 胡建宝, 阚艳梅, 陈小武, 董绍明. SiC/SiC-哈氏合金异质连接机制及其氟熔盐腐蚀特性分析[J]. 无机材料学报, 2022, 37(4): 452-458.
[6]	吴西士, 朱云洲, 黄庆, 黄政仁. 树脂基多孔碳孔结构对C_f/SiC复合材料连接性能的影响[J]. 无机材料学报, 2022, 37(12): 1275-1280.
[7]	马登浩, 侯振华, 李军平, 孙新, 金恩泽, 尹健. 界面相对3D-SiC/SiC复合材料静态力学性能及内耗特征的影响[J]. 无机材料学报, 2021, 36(1): 55-60.
[8]	张冰玉,王岭,王晓猛,邱海鹏. 不同先驱体制备C/SiC复合材料及其浸渍行为[J]. 无机材料学报, 2020, 35(9): 1017-1022.
[9]	黄喜鹏, 王波, 杨成鹏, 潘文革, 刘小瀛. 基于声发射信号的三维针刺C/SiC复合材料拉伸损伤演化研究[J]. 无机材料学报, 2018, 33(6): 609-616.
[10]	何飞, 李亚, 骆金, 方旻翰, 赫晓东. 具有气凝胶结构特征的C/SiO₂和C/SiC复合材料研究进展[J]. 无机材料学报, 2017, 32(5): 449-458.
[11]	赵爽, 杨自春, 周新贵. 不同界面SiC/SiC复合材料的断裂行为研究[J]. 无机材料学报, 2016, 31(1): 58-62.
[12]	杨晓龙, 屠恒勇, 余晴春. SUS430合金表面Co₃O₄和La_0.6Sr_0.4CoO_3-δ双层涂层的制备及性能研究[J]. 无机材料学报, 2015, 30(4): 379-384.
[13]	朱巍巍, 陈继春. 微晶玻璃焊料在连接过程中的晶化行为研究[J]. 无机材料学报, 2015, 30(12): 1310-1314.
[14]	马青松, 刘海韬, 潘余, 刘卫东, 陈朝辉. C/SiC复合材料在超燃冲压发动机中的应用研究进展[J]. 无机材料学报, 2013, 28(3): 247-255.
[15]	朱焕霞, 李克智, 卢锦花, 李贺军, 王建阳. CeO₂掺杂MAS中间层对C/C-LAS接头性能的影响[J]. 无机材料学报, 2013, 28(12): 1345-1348.