Preparation of PZT95/5 Nano-powders with Modified Sol-Gel Method

Journal of Inorganic Materials

• Research Paper • Previous Articles Next Articles

Preparation of PZT95/5 Nano-powders with Modified Sol-Gel Method

XIE Xiang-Hua¹; DONG Ya-Ming¹; YAO Chun-Hua²; QU Cui-Feng²; DONG Xian-Lin²

1.East China University of Science and Technology; Shanghai 200237 China; 2. Shanghai Institute of Ceramics Chinese Academy of Sciences; Shanghai 200050; China

Received:2002-12-30 Revised:2003-02-19 Published:2004-01-20 Online:2004-01-20

Abstract

Abstract: PbZr_0.95Ti_0.05O₃ nano-powders were synthesized with a modified sol-gel method at low calcining temperatures. Pb(CH₃COO)₂·3H₂O, Zr(NO₃)₄·5H₂O and Ti(C₄H₉O)₄ were used as parent reagents. The sol-gel method was modified by cutting down certain procedures and calcining wet gel in a proper heating sequence. XRD and TEM testy show that the PZT nano-particles are ultrafine and uniform, their diameters are around 10 nanometers.

Key words: PZT, sol-gel, nano-powders, synthesize

CLC Number:

TQ174
TM22

XIE Xiang-Hua,DONG Ya-Ming,YAO Chun-Hua,QU Cui-Feng,DONG Xian-Lin. Preparation of PZT95/5 Nano-powders with Modified Sol-Gel Method[J]. Journal of Inorganic Materials.

[1]	SHEN Bin, ZHANG Xu, XIONG Huai, LI Haiyuan, XIE Xinglong. Preparation and Optical Properties of Sol-Gel SiO₂ Antireflective Films [J]. Journal of Inorganic Materials, 2024, 39(5): 525-530.
[2]	JIANG Qiang, SHI Lizhi, CHEN Zhengran, ZHOU Zhiyong, LIANG Ruihong. Preparation and Properties of Hard PZT Piezoelectric Ceramics Poled above Curie Temperature and Multilayer Actuators [J]. Journal of Inorganic Materials, 2024, 39(10): 1091-1099.
[3]	DAI Le, LIU Yang, GAO Xuan, WANG Shuhao, SONG Yating, TANG Mingmeng, DMITRY V Karpinsky, LIU Lisha, WANG Yaojin. Self-polarization Achieved by Compositionally Gradient Doping in BiFeO₃ Thin Films [J]. Journal of Inorganic Materials, 2024, 39(1): 99-106.
[4]	JIA Yuna, CAO Xu, JIAO Xiuling, CHEN Dairong. Preparation of Alumina Ceramic Continuous Fibers with Inorganic Acidic Aluminum Sol as Precursor [J]. Journal of Inorganic Materials, 2023, 38(11): 1257-1264.
[5]	LIU Dingwei, ZENG Jiangtao, ZHENG Liaoying, MAN Zhenyong, RUAN Xuezheng, SHI Xue, LI Guorong. High Piezoelectric Property and Low Electric Field-strain Hysteresis of BiAlO₃-doped PZT Ceramics [J]. Journal of Inorganic Materials, 2022, 37(12): 1365-1370.
[6]	MAN Xin, WU Nan, ZHANG Mu, HE Hongliang, SUN Xudong, LI Xiaodong. Lu₂O₃-MgO Nano-powder: Synthesis and Fabrication of Composite Infrared Transparent Ceramics [J]. Journal of Inorganic Materials, 2021, 36(12): 1263-1269.
[7]	YANG Conggang, MI Le, FENG Aihu, YU Yang, SUN Dazhi, YU Yun. Synthesis and Performance of KH-560 Modified SiO₂ Insulation Coating [J]. Journal of Inorganic Materials, 2021, 36(12): 1343-1348.
[8]	DONG Chang, LIANG Ruihong, ZHOU Zhiyong, DONG Xianlin. Piezoelectric Property of PZT-based Relaxor-ferroelectric Ceramics Enhanced by Sm Doping [J]. Journal of Inorganic Materials, 2021, 36(12): 1270-1276.
[9]	ZHU Ben-Bi,ZHANG Wang,ZHANG Zhi-Jian,ZHANG Jian-Zhong,IMRAN Zada,ZHANG Di. Photothermal Enhanced Photocatalytic Properties of Titanium Dioxide (B)/Glass Fiber Cloth [J]. Journal of Inorganic Materials, 2019, 34(9): 961-966.
[10]	Shao-Dan ZHANG, Wei-Wei BAO, Hai-Ping MA. Near-infrared Reflective Pigments Based on Cu ²⁺ and Tb ³⁺ Codoped BaZrO₃: Preparation and Performance [J]. Journal of Inorganic Materials, 2019, 34(6): 599-604.
[11]	LIU Qian, ZHOU Zhen-Zhen. Progress in Activated-synthesis of Si-based Oxynitrides Materials at Low Temperatures [J]. Journal of Inorganic Materials, 2018, 33(2): 129-137.
[12]	NIE Heng-Chang, WANG Yong-Ling, HE Hong-Liang, WANG Gen-Shui, DONG Xian-Lin. Recent Progress of Porous PZT95/5 Ferroelectric Ceramics [J]. Journal of Inorganic Materials, 2018, 33(2): 153-161.
[13]	ZHAO Hui-Yue, WANG Xiao-Dong, FENG Jian-Bin, LIU Yuan, HUANG Ji-Chen, SHEN Jun. Environmental Stable SiO₂Antireflective Coating Modified via NH₃/HTMS Vapor Phase Treatment [J]. Journal of Inorganic Materials, 2018, 33(11): 1219-1224.
[14]	HE Fei, LI Ya, LUO Jin, FANG Min-Han, HE Xiao-Dong. Development of SiO₂/C and SiC/C Composites Featuring Aerogel Structures [J]. Journal of Inorganic Materials, 2017, 32(5): 449-458.
[15]	LU Shu-Juan, WANG Chang, ZHAO Bo-Wen, WANG Hao, LIU Jing-Bing, YAN Hui. Electrochromic Properties of PEG-modified Tungsten Oxide Thin Films [J]. Journal of Inorganic Materials, 2017, 32(2): 185-190.

Preparation of PZT95/5 Nano-powders with Modified Sol-Gel Method

PDF (PC)

Knowledge

Cited

Abstract

Cite this article

share this article

References

Related Articles 15

Recommended Articles

Metrics

Comments