Preparation of Dense BaTiO3 Ceramic Fiber by a Sol-Gel and Solvothermal Route

doi:10.3724/SP.J.1077.2006.01487

Journal of Inorganic Materials

• Research Paper • Previous Articles Next Articles

Preparation of Dense BaTiO₃ Ceramic Fiber by a Sol-Gel and Solvothermal Route

LIU Yong¹, LU Qi-Fang², CHEN Chang-Long³, CHEN Dai-Rong¹, JIAO Xiu-Ling¹

(1. Department of Chemistry, Shandong University, Jinan 250100, China; 2. Department of Materials, Shandong Institute of Light Industry, Jinan 250100, China; 3. Department of Chemistry, Jinan University, Jinan 250022, China)

Received:2005-12-19 Revised:2006-04-14 Published:2006-11-20 Online:2006-11-20

Abstract

Abstract: Dense BaTiO₃ ceramic fibers were obtained by solvothermal treatment of the green gel fibers, which were drawn from a sol using barium acetate hydrate and catechol-complexed titanium isoproposide as starting materials, at 180℃ for 12h in n-hexane following a heat process to 1100℃ with a heating rate of 1℃/min for crystallization. The as-synthesized BaTiO₃ ceramic fibers were characterized by X-ray diffraction (XRD), Infrared (IR) spectra and scanning electron microscope (SEM) techinques.

Key words: BaTiO3, ceramic fiber, sol-gel, solvothermal

CLC Number:

TQ343

LIU Yong,LU Qi-Fang,CHEN Chang-Long,CHEN Dai-Rong,JIAO Xiu-Ling. Preparation of Dense BaTiO₃ Ceramic Fiber by a Sol-Gel and Solvothermal Route
[J]. Journal of Inorganic Materials, DOI: 10.3724/SP.J.1077.2006.01487.

[1]	SHEN Bin, ZHANG Xu, XIONG Huai, LI Haiyuan, XIE Xinglong. Preparation and Optical Properties of Sol-Gel SiO₂ Antireflective Films [J]. Journal of Inorganic Materials, 2024, 39(5): 525-530.
[2]	DAI Le, LIU Yang, GAO Xuan, WANG Shuhao, SONG Yating, TANG Mingmeng, DMITRY V Karpinsky, LIU Lisha, WANG Yaojin. Self-polarization Achieved by Compositionally Gradient Doping in BiFeO₃ Thin Films [J]. Journal of Inorganic Materials, 2024, 39(1): 99-106.
[3]	JIA Yuna, CAO Xu, JIAO Xiuling, CHEN Dairong. Preparation of Alumina Ceramic Continuous Fibers with Inorganic Acidic Aluminum Sol as Precursor [J]. Journal of Inorganic Materials, 2023, 38(11): 1257-1264.
[4]	WANG Xingang, YANG Qingqing, LIN Genlian, GAO Wei, QIN Fulin, LI Rongzhen, KANG Zhuang, WANG Xiaofei, JIANG Danyu, YAN Jina. High Temperature Tensile Property of Domestic 550-grade Continuous Alumina Ceramic Fiber [J]. Journal of Inorganic Materials, 2022, 37(6): 629-635.
[5]	ZHANG Xiaoshan, WANG Bing, WU Nan, HAN Cheng, LIU Haiyan, WANG Yingde. Infrared Radiation Shielded SiZrOC Nanofiber Membranes: Preparation and High-temperature Thermal Insulation Performance [J]. Journal of Inorganic Materials, 2022, 37(1): 93-100.
[6]	ZHANG Xiaoshan, WANG Bing, WU Nan, HAN Cheng, WU Chunzhi, WANG Yingde. Micro-nano Ceramic Fibers for High Temperature Thermal Insulation [J]. Journal of Inorganic Materials, 2021, 36(3): 245-256.
[7]	MAN Xin, WU Nan, ZHANG Mu, HE Hongliang, SUN Xudong, LI Xiaodong. Lu₂O₃-MgO Nano-powder: Synthesis and Fabrication of Composite Infrared Transparent Ceramics [J]. Journal of Inorganic Materials, 2021, 36(12): 1263-1269.
[8]	YANG Conggang, MI Le, FENG Aihu, YU Yang, SUN Dazhi, YU Yun. Synthesis and Performance of KH-560 Modified SiO₂ Insulation Coating [J]. Journal of Inorganic Materials, 2021, 36(12): 1343-1348.
[9]	SUN Tuanwei,ZHU Yingjie. One-step Solvothermal Synthesis of Strontium-doped Ultralong Hydroxyapatite Nanowires [J]. Journal of Inorganic Materials, 2020, 35(6): 724-728.
[10]	ZHU Ben-Bi,ZHANG Wang,ZHANG Zhi-Jian,ZHANG Jian-Zhong,IMRAN Zada,ZHANG Di. Photothermal Enhanced Photocatalytic Properties of Titanium Dioxide (B)/Glass Fiber Cloth [J]. Journal of Inorganic Materials, 2019, 34(9): 961-966.
[11]	Shao-Dan ZHANG, Wei-Wei BAO, Hai-Ping MA. Near-infrared Reflective Pigments Based on Cu ²⁺ and Tb ³⁺ Codoped BaZrO₃: Preparation and Performance [J]. Journal of Inorganic Materials, 2019, 34(6): 599-604.
[12]	Jian-Huang KE, Kai XIE, Yu HAN, Wei-Wei SUN, Shi-Qiang LUO, Jin-Feng LIU. Morphology Controlling of the High-voltage Cathode Materials with Different Co-solvents [J]. Journal of Inorganic Materials, 2019, 34(6): 618-624.
[13]	SUI Li-Li, WANG Run, ZHAO Dan, SHEN Shu-Chang, SUN Li, XU Ying-Ming, CHENG Xiao-Li, HUO Li-Hua. Construction of Hierarchical α-MoO₃ Hollow Microspheres and Its High Adsorption Performance towards Organic Dyes [J]. Journal of Inorganic Materials, 2019, 34(2): 193-200.
[14]	ZHANG Yi-Qing, LIU Li, ZHANG Shu-Juan, WAN Zheng-Rui, LIU Hong-Ying, ZHOU Li-Qun. Preparation and Dehydrogenation Property of NH₂-UIO-66 Supported RuCuMo Nanocatalyst [J]. Journal of Inorganic Materials, 2019, 34(12): 1316-1324.
[15]	WU Nan, WAN Lynn Yuqin, WANG Ying-De, FRANK KO. Electrospun Silicon Oxycarbide Ultrafine Fibers Derived from Polycarbosilane [J]. Journal of Inorganic Materials, 2018, 33(3): 357-362.

Preparation of Dense BaTiO₃ Ceramic Fiber by a Sol-Gel and Solvothermal Route

PDF (PC)

Knowledge

Abstract

Cite this article

share this article

References

Related Articles 15

Recommended Articles

Metrics

Comments