Journal of Inorganic Materials

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CVD Method to Synthesize Carbon Nanotubes on a Large Scale

SUN Yan-Lin; ZHANG Xiao-Bin; NING Yue-Sheng; KONG Fan-Zhi; LIU Fu   

  1. Electron Microscope Laboratory of Academy of Material and Chemical Engineering; National Key Lab of Silicon; Zhejiang University; Hangzhou 310027; China
  • Received:2001-02-26 Revised:2001-04-10 Published:2002-03-20 Online:2002-03-20

Abstract: Acetylene cracked under normal pressure at 700-800℃ with active nanoscale cobalt particles as catalyst and carbon nanotubes were prepared on a large scale. The final product rate was above 50wt% after 10min growth, and also defects were almost nonexistent. The lengthes of the carbon nanotubes ranged from 5 to 30μm. Non-well distributed carbon on catalyst surface accelerated the nucleating process. The growing time limitation was about 15min and then growing process became slow.

Key words: carbon nanotubes, CVD, normal pressure, sol-gel

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