Preparation of Lead Lanthanum Zirconate Titanate Stannate Ceramics by Partial Chemical Method and Its Electric Field Induced Strain

Abstract

Abstract: A partial chemical method was developed for the synthesis of PbNb(Zr,Sn,Ti)O₃ antiferroelectric ceramics. Single perovskite phase was formed in the precursor
calcined at 600℃ for 2h and a submicron particle size distribution of calcined powder was achieved by planetary ball milling. Average grain size about
4μm and relative density greater than 97% were obtained from samples prepared by a tape-casting method and sintered at 1100℃ for 4h. In samples with
composition of Pb_0.99Nb_0.02[(Zr_0.6Sn_0.4)_1-yTi_y]_0.98O₃, there shows a increase of dielectric constant and a trend of transition from antiferroelectric
state to ferroelectric state with the increase of Ti content. A strain curve with maximum longitude strain of 0.33% under 6kV/mm electric field was measured from
samples with composition of y=0.06.

Key words: partial chemical method, antiferroelectric ceramics, electric field induced strain

CLC Number:

TN304

CHEN Ming,YAO Xi,ZHANG Liang-Ying. Preparation of Lead Lanthanum Zirconate Titanate Stannate Ceramics by Partial Chemical Method and Its Electric Field Induced Strain[J]. Journal of Inorganic Materials.

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Preparation of Lead Lanthanum Zirconate Titanate Stannate Ceramics by Partial Chemical Method and Its Electric Field Induced Strain

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