Synthesis Study of Lu3Al5O12(Ce) Nanoscaled Powder by Co-precipitation

doi:10.3724/SP.J.1077.2009.00079

Abstract

Abstract: Ce³⁺-doped Lutetium aluminum garnet Lu₃Al₅O₁₂ phosphors were prepared by an anti co-precipitation from mixing solution of lutetium, aluminum and cerium nitrates using the ammonium hydrogen carbonate as precipitate，followed by the calcination at low temperatures. TG-DTA, FTIR, XRD, TEM and Photoluminescence were used to characterize the as-prepared phosphors. The calcining temperature has distinctly influence on the particle size and the photoluminescence of the prepared Lu₃Al₅O₁₂(Ce) powders. The resulted Lu₃Al₅O_12(Ce) powder calcined at 1000℃ for 2h has an average particle size of 30nm. And its photoluminescence is the strongest among the powders calcined in the range from 850℃ to 1200℃.
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Key words: co-precipitated, Lu₃Al₅O₁₂(Ce), luminescence, nanoscaled powder

CLC Number:

O734

XIE Jian-Jun,SHI Ying,HU Yao-Ming,CHEN Qi-Wei,SHI Jian-Lin. Synthesis Study of Lu₃Al₅O₁₂(Ce) Nanoscaled Powder by Co-precipitation[J]. Journal of Inorganic Materials, DOI: 10.3724/SP.J.1077.2009.00079.

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Synthesis Study of Lu₃Al₅O₁₂(Ce) Nanoscaled Powder by Co-precipitation

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