Adv. Search
Journal of Inorganic Materials

Journal of Inorganic Materials >

2006 , Vol. 21 >Issue 5: 1079 - 1084

DOI: https://doi.org/10.3724/SP.J.1077.2006.01079

Research Paper

Preparation of Ultrafine Barium Sulfate in Impinging Streams Microreactor

  • WU Guo-Hua ,
  • ZHOU Hong-Zhao ,
  • ZHU Shen-Lin
Expand
  • Department of Chemical Engineering, State Key Laboratory of Chemical Engineering, Tsinghua University, Beijing 100084, China

Received date: 2005-09-19

  Revised date: 2005-12-23

  Online published: 2006-09-20

Fold

Abstract

PAANH4 was used as dispersant to improve the dispersibility of particles. The velocity and angle of the impinging streams were investigated to obtain the optimum conditions. Ultrafine barium sulfate particles were prepared in the impinging streams microreactor. The ultrafine particles were characterized by XRD, TEM, and BET. The results indicate that micromixing and homogeneous supersaturation of the reaction are enhanced by impinging streams. The product is obtained as particles with mean size of 100nm and specific surface area of 60m2·g-1.

Key words： impinging streams; microreactor; ultrafine barium sulfate

Cite this article

WU Guo-Hua , ZHOU Hong-Zhao , ZHU Shen-Lin . Preparation of Ultrafine Barium Sulfate in Impinging Streams Microreactor[J]. Journal of Inorganic Materials, 2006 , 21(5) : 1079 -1084 . DOI: 10.3724/SP.J.1077.2006.01079

References

[1] Qi L M, Ma J M, et al. Colloids and Surfaces, 1996, 108: 117--126.
[2] Gan L M, Zhang L H, et al. Material Chemistry and Physics, 1995, 40: 94--98.
[3] 周鸿顺, 杨荣榛(ZHOU Hong-shun, et al). 陕西师范大学学报(自然科学版) (Journal of Shanxi Normal University(Natural Science Edition)), 1998, 26(3): 71--73.
[4] 王晓辉, 蒋斌波, 陈纪忠(WANG Xiao-hui, et al). 无机材料学报(Journal of Inorganic Materials), 2005, 20(4): 801--807.
[5] Mark S, Julian E, Sean D. Langmuir, 2002, 18(12): 5023--5026.
[6] Chen G G, Luo G S. Powder Technology, 2004, 139: 180--185.
[7] UCHIDA M, SUE A. Journal of Mater. Sci. Lett., 2002, 15: 1373--1374.
[8] Chen J F, Shen Z G, Liu F T. Scripta Materialia, 2003, 49(6): 509--514.
[9] Wang S J, Devahastin S, Mujumdar A S. Applied Thermal Engineering, 2005, 25: 253--269.
[10] Zhou H Z, Wu G H, Zhu S L. 2nd Chinese National Chemical and Biochemical Engineering Annual Meeting, Peking, China, 2005.
[11] 张立德. 超微粉体制备与应用技术, 第一版. 北京: 中国石化出版社, 2001. 237--239.
[12] 徐华蕊, 李凤生, 陈舒林, 等(XU H R, et al). 化工进展(Chemical Industry and Engineering Progress), 1996, (5): 29--31.
[13] 周洪兆, 朱慎林(ZHOU H Z, et al). 机械工程材料(Materials for Mechanical Engineering), 2005, 29(4): 17--19.
Options
Outlines

/

〈 〉