Research Paper

Synthesis Study of Lu3Al5O12(Ce) Nanoscaled Powder by Co-precipitation

  • XIE Jian-Jun ,
  • SHI Ying ,
  • HU Yao-Ming ,
  • CHEN Qi-Wei ,
  • SHI Jian-Lin
Expand
  • 1. School of Materials Science and Engineering, Shanghai University, Department of Electronics and Information Materials, Shanghai 200072, China; 2. Research Center of Analysis and Measurement, Shanghai Fudan University, Shanghai 200433, China; 3.Shanghai Institute of Ceramics, Chinese Academy of Sciences, Shanghai 200050, China

Received date: 2008-04-09

  Revised date: 2008-06-11

  Online published: 2009-01-20

Abstract

Ce3+-doped Lutetium aluminum garnet Lu3Al5O12 phosphors were prepared by an anti co-precipitation from mixing solution of lutetium, aluminum and cerium nitrates using the ammonium hydrogen carbonate as precipitate,followed by the calcination at low temperatures. TG-DTA, FTIR, XRD, TEM and Photoluminescence were used to characterize the as-prepared phosphors. The calcining temperature has distinctly influence on the particle size and the photoluminescence of the prepared Lu3Al5O12(Ce) powders. The resulted Lu3Al5O12(Ce) powder calcined at 1000℃ for 2h has an average particle size of 30nm. And its photoluminescence is the strongest among the powders calcined in the range from 850℃ to 1200℃.

Cite this article

XIE Jian-Jun , SHI Ying , HU Yao-Ming , CHEN Qi-Wei , SHI Jian-Lin . Synthesis Study of Lu3Al5O12(Ce) Nanoscaled Powder by Co-precipitation[J]. Journal of Inorganic Materials, 2009 , 24(1) : 79 -82 . DOI: 10.3724/SP.J.1077.2009.00079

References

[1]van Eijk C W E. Nucl. Instr. Meth. A , 1997,392(2): 285-290. 
[2]Lempicki A, Randles M H, Wisniew ski D, et al. IEEE Trans. Nucl. Sci., 1995, 429(4): 280-284. 
[3]van Eijk C W E, Andriessen J, Dorenbos P, et al., Nucl. Instr. Meth. A, 1994, 348(2-3): 546-550. 
[4]Nikl M, Mihokova E, Mares J A, et al. Phys. Stat. Sol. (a), 2000,181: R10-R12.
[5]Ogino H, Yoshikawa A, Lee J H, et al. J. Cryst. Growth, 2003, 253(3): 314-318.
[6]Yoshikawa A, Nikl M, Ogino H, et al. J. Cryst.Growth, 2003,250(1): 94-99.
[7]Yoshikawa A, Ogino H, Lee J H, et al. Opt. Mater.,2003, 24(2): 275-279. 
[8]Manalert R, Rahaman M N. J. Mater. Sci.,1996,31(13): 3453-3458. [9]Tachiwaki T, Yoshinaka M, Hirota K, et al. Solid State Comm., 2001, 119(11):603-606. 
[10]Kinsman K M, Mckittrick J, Sluzky E, et al. J. Am. Ceram. Soc., 1994,77(11): 2866-2872.
[11]Li J G, Ikegami T, Lee J H, et al. J. Eur. Ceram. Soc., 2000, 20(14): 2395-2405.
[12]Vrolijk J W G A, Metselaar R. Homogeneous coprecipitation of precursor for preparation of yttrium aluminum garnet, in: P. Vincenzini (Ed.), Ceramics Today - Tomorrow’s Ceramics, Elsevier Science Publishers, Amsterdam, 1991: 935-941. 
[13]Pillai K T, Kamat R V, Vaigya V N, et al. Mater. Chem. Phys., 1996, 44(3): 255-260.
[14]Shea L E, Mckittrick J, Lopez O A, et al. J. Am. Ceram. Soc., 1996, 79(12): 3257-3265. 
[15]Hayashi K, Toyoda S, Takebe H, et al. J. Ceram. Soc. Jpn., 1991, 99(7): 550-555.
[16]Dean J A. LANGE’s Handbook of Chemistry(兰氏化学手册),第15版. [17]杭州大学化学系分析化学教研室.分析化学手册(第二分册)分析化学,第二版. 北京:化学工业出版社,1997.
[18]Jiang D Y , Wang Z L, Zhang F L, et al. J.Mater.Res., 1998, 13(10): 2950-2955.
Outlines

/