The sintering characters and phase composition of BaO-CeO2-TiO2 were examined with TG-DTA, SEM, EDAX and XRD. The pretreating temperature and sintering temperature were 900--1100℃ and 1250--1300℃,respectively. The results indicate that the samples Ba 6-3x Ce 8+2x Ti 18 O54(x=0.8) sintered at 1300℃ consist of A and B phases, whose elements molar ratio are Ce:O=1.0:1.3 and Ba:Ti:Ce: O=1.00:6.70:0.35:9.46 respectively. And the above sintered samples with permittivity of 28.72 have the highest quality factor of 4862.13GHz.
ZHOU Dong-Xiang
,
YU Xiao-Hua
,
WANG He
,
ZHAO Jun
. Sintering Characters and Phase Composition of BaO-CeO2-TiO2 Microwave Dielectric Ceramics[J]. Journal of Inorganic Materials, 2007
, 22(6)
: 1197
-1200
.
DOI: 10.3724/SP.J.1077.2007.01197
[1] Guha J P, Kolar D. J. Am. Ceram. Soc., 1973, 56 (1): 5--8.
[2] Rawn C J, Makovec D, Golic L, et al. Mater. Res. Bull., 1997, 32 (12): 1657--1672.
[3] Sreemoolanadhan H, Sebastian M T, Ratheesh R, et al. J. Solid State Chem., 2004, 177: 3995--4000.
[4] Mudrodubova L P, Lisker K E, Totenberg B A, et al. Ser. Radiodet. Radiokomp., 1982, 1: 3--8.
[5] Hoffmann C, Waser R. Ferroelectrics, 1997, 201: 127--135.
[6] Hennings D F K, Schreinemacher B, Schreinemacher H. J. Euro. Ceram. Soc., 1994, 13 (1): 81--88.