Chemical Reduction Synthesis of Hexagonal B-C-N Compound

doi:10.3724/SP.J.1077.2008.01067

Abstract

Abstract: Hexagonal B-C-N compounds were successfully synthesized by using hydrogen-free 1,3,5-trichlorotriazine and boron tribromide as reactants and metal sodium as reluctant through a chemical reduction synthesis method at 450℃. The synthesized sample was characterized by X-ray diffraction (XRD), transmission electron microscope (TEM), selected area electron diffraction (SAED), electron energy loss spectroscope (EELS) and Fourier transformation infrared spectroscope (FTIR), respectively. The results indicate that the synthesized B-C-N compound is polycrystalline with hexagonal structure and its composition is B_0.5C_0.07N_0.43.

Key words: hexagonal B-C-N compound, chemical reduction synthesis method, X-ray diffraction, electron energy loss spectroscopy

CLC Number:

O613

SUN Guang,WU Qing-Hua,HU Qian-Ku,YU Dong-Li. Chemical Reduction Synthesis of Hexagonal B-C-N Compound[J]. Journal of Inorganic Materials, DOI: 10.3724/SP.J.1077.2008.01067.

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Chemical Reduction Synthesis of Hexagonal B-C-N Compound

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