钨酸铅晶体生长及其组份挥发

无机材料学报

钨酸铅晶体生长及其组份挥发

廖晶莹; 沈炳孚; 邵培发; 殷之文

中国科学院上海硅酸盐研究所; 上海200050

收稿日期:1996-01-25 修回日期:1996-03-22 出版日期:1997-06-20 网络出版日期:1997-06-20

Growth and Composition Evaporated of Lead Tungstate Crystals

LIAO Jingying; SHEN Bingfu; SHAO Peifa; YIN Zhiwen

Shanghai Institute of Ceramics; Chinese Academy of Sciences Shanghai 200050 China

Received:1996-01-25 Revised:1996-03-22 Published:1997-06-20 Online:1997-06-20

摘要/Abstract

摘要： 本文首次报道了用坩埚下降技术生长钨酸铅（PWO）晶体；研究了提拉和坩埚下降两种技术生长PWO晶体的组份挥发，得到的结果是PbO的挥发速率高于WO₃，并对一组晶体不同部位的X射线发光性能作了研究．

关键词: 钨酸铅晶体, 坩埚下降技术, 组份挥发, X线发光性能

Abstract: This paper described PWO crystals grown by Bridgman technology for the first time. Thematerials evaporated from the PbWO₄ melt were studied during tile growth of PWO crystals bymeans of both Czochralski and Bridgman mcthod. The results indicated that the evaporation rateof PbO is higher than that of WO₃. Further the X-ray luminescence properties were investigatedof different positions of PWO crystals.

Key words: lead tungstate crystal, Bridgman technology, composition evaporated, X-ray luminescence property

廖晶莹,沈炳孚,邵培发,殷之文. 钨酸铅晶体生长及其组份挥发[J]. 无机材料学报.

LIAO Jingying,SHEN Bingfu,SHAO Peifa,YIN Zhiwen. Growth and Composition Evaporated of Lead Tungstate Crystals[J]. Journal of Inorganic Materials.

[1]	张昕,廖晶莹,袁辉,沈炳孚,邵培发,李长泉,殷之文. Y³⁺:PbWO₄晶体低剂量辐照行为研究[J]. 无机材料学报, 2002, 17(3): 448-454.
[2]	杨培志,廖晶莹,沈炳孚,邵培发,倪海红,方全兴,殷之文. 高质量钨酸铅(PWO)晶体的生长[J]. 无机材料学报, 2002, 17(2): 210-214.
[3]	黄红伟,DONG Ming,YE Zuo-Guang,冯锡淇. 钆掺杂钨酸铅闪烁晶体的介电双弛豫峰研究[J]. 无机材料学报, 2002, 17(1): 29-34.
[4]	廖晶莹,沈炳孚,邵培发,殷之文. PbWO₄晶体的热膨胀及坩埚下降技术生长晶体开裂分析[J]. 无机材料学报, 1997, 12(2): 228-230.