无机材料学报

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化学气相渗透2D SiC/SiC窄带随机振动疲劳损伤与性能退化

刘明扬1(), 王纯2, 程鹏飞2, 马雪寒1, 高祥云3, 由博杰1, 赵录峰4, 成来飞1,4, 张毅1,*()   

  1. 1 西北工业大学 超高温结构复合材料重点实验室西安 710072
    2 中国飞机强度研究所西安 710065
    3 西安航空制动科技有限公司西安 713106
    4 西安鑫垚陶瓷复合材料股份有限公司西安 710051

2D SiC/SiC Manufactured by Chemical Vapor Infiltration: Narrow Band Random Vibration Fatigue Damage and Performance Degradation

LIU Mingyang1(), WANG Chun2, CHENG Pengfei2, MA Xuehan1, Gao Xiangyun3, YOU Bojie1, ZHAO Lufeng4, CHENG Laifei1,4, ZHANG Yi1,*()   

  1. 1 National Key Laboratory of Thermostructural Composite Materials, Northwestern Polytechnical University, Xi’an 710072, China
    2 AVIC Aircraft Strength Research Institute, Xi'an 710065, China
    3 Xi'an Aviation Brake Technology Co., Ltd, Xi'an 713106, China
    4 Xi'an Xinyao Ceramic Composite Material CO., LTD., Xi’an 710051, China

摘要:

随着航空发动机热端部件对高温性能与轻量化的要求日益严苛,SiC/SiC复合材料凭借其优异的耐高温性、低密度和耐腐蚀性,成为极具应用潜力的替代材料。然而,服役过程中不可避免地承受复杂振动载荷,振动引发的疲劳损伤已成为限制其工程应用的关键问题。本工作采用化学气相渗透法制备了2D SiC/SiC板材,并加工成两侧具有圆弧状缺口的试样,在一阶振型下开展了窄带随机振动疲劳试验,系统揭示其损伤演化过程及拉伸性能退化规律。研究结果表明,随等效应力 σ e增大,2D SiC/SiC板结构的归一化全时域曲线整体向下偏移,低应力区的响应表现出显著的分散性。基于微结构图像分析,2D SiC/SiC板结构的损伤演化可分为三阶段:基体损伤阶段、界面损伤阶段和纤维损伤阶段,损伤速率呈现“快-慢-快”的变化趋势。残余拉伸性能结果表明,2D SiC/SiC板结构的拉伸性能呈指数型下降趋势,当共振频率降幅为31.9%时,其拉伸强度、比例极限应力、弹性模量和回弹模量分别下降至270.0 MPa、64.1 MPa、106.3 GPa和0.020 MJ/m3,均不足制备态性能的70%。拉伸断口形貌分析表明,基体裂纹和纤维磨损是导致拉伸性能退化的关键因素。本研究为评估2D SiC/SiC板结构在振动环境下的服役可靠性提供了重要依据和实验支撑。

关键词: 2D SiC/SiC, 随机振动, 疲劳损伤, 等效应力, 拉伸性能

Abstract:

The operational requirements for high-temperature performance and structural weight reduction in aero-engine hot section components continue to intensify under demanding service conditions. Silicon carbide fiber reinforced silicon carbide matrix (SiC/SiC) composites are widely recognized as exceptionally promising alternative materials owing to their outstanding high-temperature stability, substantially reduced density, and superior corrosion resistance characteristics. However, under actual service enviroments, these composites inevitably experience complex vibrational loading spectra, with the consequent vibration induced fatigue damage accumulation emerging as a critical limiting factor in their practical engineering implementation. In this study, 2D SiC/SiC plates were fabricated by chemical vapor infiltration. Specimens featuring bilateral arc-shaped notches were machined from the plates and subsequently subjected to narrow band random vibration fatigue tests under the first order vibration mode. This experimental approach was undertaken specifically to investigate the progressive damage evolution process and the accompanying degradation patterns in tensile properties exhibited by the 2D SiC/SiC plate structure under vibrational fatigue loading. The research findings reveals that the normalized full time-domain characteristic curves of the 2D SiC/SiC plate structures exhibit progressive downward displacement as the applied equivalent stress amplitude (σe) increases. These curves concurrently manifest pronounced statistical dispersion throughout the low stress loading regime. Microstructural analyses enable the classification of the damage evolution within the 2D SiC/SiC plate structure into three distinct, sequential stages: the initial matrix damage stage, the subsequent interface damage stage, and the final fiber damage stage. Quantitatively, the damage progression rate follows a distinct three stage evolution—commencing with rapid progression, transitioning to reduced propagation velocity, and culminating in accelerated damage advancement during the terminal phase.The residual tensile properties demonstrate that the tensile characteristics of the 2D SiC/SiC plate structure follow an exponential decline trend. At a resonance frequency reduction of 31.9%, the tensile strength, proportional limit stress, elastic modulus, and resilience modulus have degraded to 270.0 MPa, 64.1 MPa, 106.3 GPa, and 0.020 MJ/m³, respectively — all falling below 70% of the corresponding values in the as-fabricated, pristine state. Subsequent analyses of the tensile fracture surface reveal matrix cracking and pronounced fiber wear as the dominant damage mechanisms responsible for the significant degradation observed in the tensile properties of the vibration fatigued composite structure. These findings provide critical experimental basis for assessing the service reliability of 2D SiC/SiC plate structures under vibrational service conditions.

Key words: 2D SiC/SiC, random vibration, fatigue damage, equivalent stress, tensile properties

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