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Journal of Inorganic Materials

Journal of Inorganic Materials >

2007 , Vol. 22 >Issue 1: 40 - 44

DOI: https://doi.org/10.3724/SP.J.1077.2007.00040

Research Paper

Preparation of Different Topography NiCo2O4 with Surfactant by Solid

  • ZHUANG Jia ,
  • CHI Yan-Hua ,
  • WANG Dong
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  • 1. Institute of Materials Science and Engineering, Southwest Petroleum University, Chengdu 610500, China; 2. Institute of Materials Science and Engineering, Southwest University of Science and Technology, Mianyang 621002, China

Received date: 2006-02-08

  Revised date: 2006-04-11

  Online published: 2007-01-20

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Abstract

Manifold mixed precursors were prepared with Ni(CH3COO)2·4H2O, Co(CH3COO)2·4H2O, H2C2O4·2H2O and different surfactants by solid state reaction at room temperature; then they were put into a bain-marie to keep 2d at 60℃. After these precursors analyzed by TG-DTA, and decomposed at 610℃, the phase and topography of the thermolysis products were characterized by XRD, SEM. The nanometer composite oxide NiCo2O4 with different topography was obtained. The experimental results show that these surfactants act as soft-templates, they have evident effect on topography of products.

Key words： NiCo2O4; surfactant; solid state reaction; topography

Cite this article

ZHUANG Jia , CHI Yan-Hua , WANG Dong . Preparation of Different Topography NiCo2O4 with Surfactant by Solid[J]. Journal of Inorganic Materials, 2007 , 22(1) : 40 -44 . DOI: 10.3724/SP.J.1077.2007.00040

References

[1] Peng Cheng-Hsium, Hwang Chyi-Ching, Wan Jun, et al. Mater. Sci. Eng. B, 2005, (117): 27--36.
[2] 陈敏, 罗孟飞, 袁贤鑫. 石油化工, 1997, 26 (6): 358--360.
[3] 蔡乃才, 张克立, 袁继兵, 等. 应用化学, 1998, 15 (6): 74--76.
[4] 陈敏, 罗孟飞, 袁贤鑫. 化学研究与应用, 1997, 9 (3): 230--234.
[5] 刘坚, 赵震, 徐春明, 等. 中国稀土学报, 2005, 23 (2): 133--137.
[6] 张高良. 工业催化剂的生产, 第一版. 上海: 上海科技出版社, 1988. 36--38.
[7] 姜国华, 姜继森(JIANG Guo-Hua, et al). 无机材料学报(Journal of Inorganic Materials), 2005, 20 (5): 1066--1070.
[8] 陈名海, 高濂(CHMING Ming-Hai, et al). 无机材料学报(Journal of Inorganic Materials), 2005, 20 (6): 1343--1348.
[9] Li Zhaofei, Li Gaobao, Sun Junliang, et al. J. Solid State Chem., 2005, (178): 3315--3322.
[10] Kim Dong Ho, Woo S I, Moon S H, et al. Solid State Commun, 2005, (136): 554--558.
[11] Ye X R, Jia D Z, Xin X Q, et al. Adv. Mater., 1999, (11): 941--942.
[12] 陈学平, 庄稼, 迟燕华, 等. 无机化学学报, 2005, 21 (3): 337--343.
[13] 庄稼, 迟燕华, 王曦(ZHUANG Jia, et al). 无机材料学报(Journal of Inorganic Materials), 2001, 16 (6): 1203--1206.
[14] 葛炜玮, 金春飞, 忻新泉. 中国化学会低热固相化学反应研讨会论文集. 郑州, 2003年11月. 72--75.

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