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Journal of Inorganic Materials

Journal of Inorganic Materials >

2008 , Vol. 23 >Issue 5: 1067 - 1069

DOI: https://doi.org/10.3724/SP.J.1077.2008.01067

Research Paper

Chemical Reduction Synthesis of Hexagonal B-C-N Compound

  • SUN Guang ,
  • WU Qing-Hua ,
  • HU Qian-Ku ,
  • YU Dong-Li
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  • 1. Institute of Materials Science and Engineering, Henan Polytechnic University, Jiaozuo 454000, China; 2. State Key Laboratory of Metastable Materials Science and Technology, Yanshan University, Qinhuangdao 066004, China

Received date: 2007-10-08

  Revised date: 2007-11-19

  Online published: 2008-09-20

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Abstract

Hexagonal B-C-N compounds were successfully synthesized by using hydrogen-free 1,3,5-trichlorotriazine and boron tribromide as reactants and metal sodium as reluctant through a chemical reduction synthesis method at 450℃. The synthesized sample was characterized by X-ray diffraction (XRD), transmission electron microscope (TEM), selected area electron diffraction (SAED), electron energy loss spectroscope (EELS) and Fourier transformation infrared spectroscope (FTIR), respectively. The results indicate that the synthesized B-C-N compound is polycrystalline with hexagonal structure and its composition is B0.5C0.07N0.43.

Key words： hexagonal B-C-N compound; chemical reduction synthesis method; X-ray diffraction; electron energy loss spectroscopy

Cite this article

SUN Guang , WU Qing-Hua , HU Qian-Ku , YU Dong-Li . Chemical Reduction Synthesis of Hexagonal B-C-N Compound[J]. Journal of Inorganic Materials, 2008 , 23(5) : 1067 -1069 . DOI: 10.3724/SP.J.1077.2008.01067

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