A MoSi2-SiC-Si coating was prepared by in situ reaction method. The phase composition and microstructure of the coating were studied by using XRD,SEM and EDS analysis, and then the anti-oxidation property of the coating was investigated. The results show that the thickness of obtained coating is about 120μm, and the main phases are composed of MoSi2, SiC and Si. The MoSi2-SiC-Si coating has excellent anti-oxidation property, which can protect Cf/SiC composites from oxidation at 1500℃ in air for 96h, the weight loss of the coated samples is only 1.8%. The weight loss of the coated Cf/SiC composites samples is primarily due to the reaction of Cf/SiC composites substrate and oxygen diffusing through the penetration cracks in the coating.
WU Ding-Xing
,
DONG Shao-Ming
,
ZHANG Xiang-Yu
,
DING Yu-Sheng
,
WANG Zhen
,
ZHOU Hai-Jun
. Preparation of MoSi2-SiC-Si Coatings for Cf/SiC Composites by in situ Reaction Method[J]. Journal of Inorganic Materials, 2009
, 24(5)
: 978
-982
.
DOI: 10.3724/SP.J.1077.2009.00978
[1]曾燮榕, 郑长卿, 李贺军, 等. 复合材料学报, 1997,14(3):37-40.
[2]Cook J, Khan A, Lee E. Materials Science and Engineering, 1992, 155(1/2):183-198.
[3]杨 鑫, 邹艳红, 黄启忠, 等(Yang Xin, et al). 无机材料学报(Journal of Inorganic Materials), 2008, 23(4):779-783.
[4]Li He-Jun, Xue Hui, Wang Yong-Jie, et al. Surface & Coating Technology, 2007, 201(24):9444-9447.
[5]Zhao Juan, Guo Quangui, Shi Jingli, et al. Surface & Coating Technology, 2006, 201(3/4):1361-1865.
[6]Nowotny H, Parthe E, Kieffer R, et al. Monatshefte fur Chemie, 1954, 85(1):255-272.
[7]Chawla K K. Reactively Sintered Molybdenum DisilicideBased Composites. VA22227, 1997.
[8]Lai Z H, Zhu J C, Jeon J H, et al. Materials Science and Engineering A, 2009, 499(1/2):267-270.