Preparation of  SnO2 Nanowires by AC Electrodeposition in Anodic Alumina Template and Its Deposition Conditions

Journal of Inorganic Materials

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Preparation of SnO₂ Nanowires by AC Electrodeposition in Anodic Alumina Template and Its Deposition Conditions

CHEN Yan-Hui¹, ZHANG Xing-Tang¹, XUE Zhong-Hui¹, DU Zu-Liang¹, LI Tie-Jin²

1. Key Lab for Special Functional Materials, Henan University, Kaifeng 475001, China; 2. Department of Chemistry, Jilin University, Changchun
130021, China

Received:2003-12-01 Revised:2004-02-23 Published:2005-01-20 Online:2005-01-20

Abstract

Abstract: By using the anode oxidation method, porous alumina anode oxidation templates (AAo) with a pore diameter of 30～50nm were
prepared, and metal tin nanowires electrodeposited in the pores of AAO, then the AAO with tin nanowires annealed in muffle in air at 750℃
for 10h, and SnO₂ nanowires formed. The effects of electrodeposition conditions, such as frequency, voltage, on the filling ratio of tin were also studied. SEM, TEM, XRD results show
that these polycrystalline SnO₂ nanowires have a diameter of 30～50nm, voltage and frequency are the key factors affecting the electrodeposition results.

Key words: SnO₂ nanowire, AAO, AC electrodepositon

CLC Number:

O646

CHEN Yan-Hui,ZHANG Xing-Tang,XUE Zhong-Hui,DU Zu-Liang,LI Tie-Jin. Preparation of SnO₂ Nanowires by AC Electrodeposition in Anodic Alumina Template and Its Deposition Conditions[J]. Journal of Inorganic Materials.

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Preparation of SnO₂ Nanowires by AC Electrodeposition in Anodic Alumina Template and Its Deposition Conditions

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