Mechanochemical Synthesis of Nanocrystalline Ni-Zn Ferrite

Journal of Inorganic Materials

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Mechanochemical Synthesis of Nanocrystalline Ni-Zn Ferrite

JIANG Ji-Sen; GAO Lian; GUO Jing-Kun; YANG Xie-Long⁺

State Key Lab on High Performance Ceramics and Saperfine Microstrvcture; Shanghai Institute ofCeramics; Chinese Academy of Sciences Shanghai 200050 China ; ⁺Department of Physics; East China Normal University Shanghai 200062 China

Received:1997-09-01 Revised:1997-09-26 Published:1998-06-20 Online:1998-06-20

Abstract

Abstract: Nanocrystalline Ni-Zn ferrite was synthesized by mechanochemical reaction from α-Fe₂O₃,ZnO and NiO powders through high energy ball milling. The synthesized samples were characterized by XRD, TEM and Mossbauer spectroscopy. The results showed that the as-millednanocrystalline size was about 5~20 um, which exhibited superparamagnetism, and the size ofthe nanocrystallite after annealed at 800℃ for 2h increased to about 50 um, which exhibitedferrimagnetism

Key words: mechanochemical synthesis, nanocrystalline, Ni-Zn ferrite

CLC Number:

TF123

JIANG Ji-Sen,GAO Lian,GUO Jing-Kun,YANG Xie-Long. Mechanochemical Synthesis of Nanocrystalline Ni-Zn Ferrite[J]. Journal of Inorganic Materials.

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Mechanochemical Synthesis of Nanocrystalline Ni-Zn Ferrite

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