Synthesis of Ti3SiC2 by Spark Plasma Sintering (SPS) with the Addition of Aluminium

Journal of Inorganic Materials

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Synthesis of Ti₃SiC₂ by Spark Plasma Sintering (SPS) with the Addition of Aluminium

ZHU Jiao-Qun; MEI Bing-Chu; CHEN Yan-Lin

State Key Lab of Advanced Technology for Materials Synthesis and Processing; Wuhan University of Technology; Wuhan 430070; China

Received:2002-05-20 Revised:2002-09-13 Published:2003-05-20 Online:2003-05-20

Abstract

Abstract: Ti₃SiC₂ material with high purity and density was fabricated by the spark plasma sintering with the addition of aluminium. The proper addition of Al accelerates the synthesis reaction and the crystal growth of Ti₃SiC₂, and increases the purity of synthesized samples. At the heating rate of 80℃/min and under the pressure of SOMPa, the ideal synthesis temperature ranges from 1150℃ to 1250℃. Ti₃SiC₂obtained is in plane-shape with the size of 5-25μm.

Key words: 铝, Ti3SiC₂, 制备, 放电等离子烧结

CLC Number:

TF123

ZHU Jiao-Qun,MEI Bing-Chu,CHEN Yan-Lin. Synthesis of Ti₃SiC₂ by Spark Plasma Sintering (SPS) with the Addition of Aluminium[J]. Journal of Inorganic Materials.

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Synthesis of Ti₃SiC₂ by Spark Plasma Sintering (SPS) with the Addition of Aluminium

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