无机材料学报

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添加AlN对FePt薄膜结构和磁性的影响

李小丽; 许小红; 武海顺   

  1. 山西师范大学化学与材料科学学院, 临汾 041004
  • 收稿日期:2004-10-15 修回日期:2004-12-06 出版日期:2005-11-20 网络出版日期:2005-11-20

Eifect of AIN on the Structure and Magnetic Properties of FePt Thin Films

LI Xiao-Li; XU Xiao-Hong; WU Hai-Shun   

  1. School of Chemistry and Material Science. Shanxi Normal University. Linfen 041004, China
  • Received:2004-10-15 Revised:2004-12-06 Published:2005-11-20 Online:2005-11-20

摘要: 采用射频磁控溅射制备了FePt(50nm)和[FePt(2,3,5nm)/AlN(1nm)]n膜,之后在550℃退火30min,研究了周期数(n)和AlN含量对[FePt/AlN]n系列多层膜结构及磁性的影响.结果表明,多层膜的矫顽力和矩形比均在n=8时出现较大值;周期数的增大会引起晶粒尺寸的长大;AlN的加入不但可以抑制FePt粒子的长大,使晶粒体积(Vgrain)和磁激活体积(V*)趋于一致,而且还能有效地降低晶粒间交换耦合作用,并且AlN含量越大,晶粒间交换耦合作用的程度越弱.

关键词: FePt/AlN薄膜, 矫顽力, 磁激活体积, 交换耦合作用

Abstract: FePt(50nm) and [FePt(2,3,5nm)/AlN(1nm)]n films were prepared by RF magnetron sputtering technique, then annealed at 550℃ for 30min. The effect of the number of bilayer repetitions (n) and AlN content on
structure and magnetic properties of various FePt/AlN multilayers was studied. The highest coercivity and squareness of FePt/AlN multilayers annealed at 550℃ were obtained for n=8. The grain size of the FePt/AlN
films by post-annealing increases with increasing n. Introducing the nonmagnetic AlN not only hinders the growth of FePt particles, but also reduces the intergrain exchange interactions of the FePt/AlN films. And the
interactions are decreased as AlN content is increased. Grain size (Vgrain) has almost the same size as magnetic activation volume (V*) due to the addition of AlN in films by post-annealing.

Key words: FePt/AIN thin film, coercivity, activation volume, exchange interaction

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