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三元层状材料结构调控及性能研究进展
丁浩明1,2,3(), 李勉1,3, 李友兵1,3, 陈科1,3, 肖昱琨1,3, 周洁4, 陶泉争4, 尹航5, 柏跃磊5, 张毕堃6, 孙志梅6, 王俊杰7, 张一鸣1,3, 黄振莺8, 张培根9, 孙正明9, 韩美康10, 赵双11, 王晨旭11, 黄庆1,3()
Progress in Structural Tailoring and Properties of Ternary Layered Ceramics
DING Haoming1,2,3(), LI Mian1,3, LI Youbing1,3, CHEN Ke1,3, XIAO Yukun1,3, ZHOU Jie4, TAO Quanzheng4, Johanna Rosen4, YIN Hang5, BAI Yuelei5, ZHANG Bikun6, SUN Zhimei6, WANG Junjie7, ZHANG Yiming1,3, HUANG Zhenying8, ZHANG Peigen9, SUN Zhengming9, HAN Meikang10, ZHAO Shuang11, WANG Chenxu11, HUANG Qing1,3()

图3. 不同的MXene的制备方法

Fig. 3. Different methods for the synthesis of MXene
(a) Schematic illustration of preparing MXene using HF solution as etchant[28]; (b) SEM image of Ti3C2Tx prepared by HF solution, showing the typical accordion-like morpholorgy of MXene particle[28]; (c) STEM image of Ti3C2Cl2 prepared by Lewis-acidic-molten-salt route, and its corresponding atomic model[24]; (d) Schematic illustration of preparing Ti3C2Tx MXene via a reaction between Ti3SiC2 and CuCl2; (e) Redox potential/Gibbs free energy between Lewis acid cations and A-site atoms in molten salts[30]; (f) Schematic illustration of the electrochemistry etching strategy for the preparation of MXene in molten salt[72]