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柔性有机硅气凝胶的制备及其高温无机化转变研究
罗艺1(), 夏书海2, 牛波2, 张亚运2, 龙东辉2()
Preparation and High Temperature Inorganic Transformation of Flexible Silicone Aerogels
LUO Yi1(), XIA Shuhai2, NIU Bo2, ZHANG Yayun2, LONG Donghui2()

图1. 溶胶-凝胶过程示意图(a), 气凝胶样品的红外谱图(b)、核磁谱图(c)和SEM照片(d~g)

Fig. 1. Schematic diagram of Sol-Gel process (a), IR spectra (b), NMR spectra (c) and SEM images (d-g) of aerogel samples
Molar ratios of VTMS/VMDMS for aerogels (d-g) are 1, 2, 3, 4, respectively