Using ethanol as the precursor of pyrolytic carbon, chemical vapor infiltration of a carbon fiber felt with an initial bulk density of 0.47g/cm3 was performed at the temperature of 1125°C and the pressure of 20kPa, resulting in a bulk density of 1.67g/cm3 after densification of 114h. Extinction angles from 19.5° to 20.5° for various regions in the densified sample are determined, which correspond to a high-textured carbon, leading to flexure strength of 137MPa. Analysis of 2D texture distribution suggests that ethanol is a promising carbon source to synthesize carbon-carbon composites with homogeneously high-textured pyrolytic carbon.
ZHANG Shou-Yang
,
YAN Xia-Feng
,
LI He-Jun
,
LI Wei
,
GUO Ling-Jun
. Deposition of Pyrolytic Carbon using Ethanol as Precursor in Chemical Vapor Infiltration[J]. Journal of Inorganic Materials, 2009
, 24(5)
: 1073
-1076
.
DOI: 10.3724/SP.J.1077.2009.09156
[1] Zhang WG, Hu ZJ, Hüttinger KJ. Carbon,2002,40 (14): 2529–2545.
[2] Delhaès P. World of carbon, volume 2: Fibers and composites. Taylor & Francis Group. 2003: 75-111.
[3] Delhaès P, Trinquecoste M, Lines JF. Carbon,2005,43(4): 681-691.
[4] Li J, Kazakov A, Frederick L. Dryer. Int. J. Chem. Kinet.,2001,33 (12): 859–867.
[5] Gong QJ, Li HJ, Li KZ. Mater. Rev.,2004,18 (9): 43-46.
[6] Huang LH, Li HJ, Hu ZB. J. Mater. Sci. Eng., 2005,9(5): 487-490.
[7] Drescher M, Hüttinger KJ, Dormann E. Carbon,2003,41 (4): 773-783.
[8] Zhang WG, Huttinger KJ. Carbon,2003,41 (4): 2325-2337.
[9] Kim DG, Kweon DW, Lee JY. J. Mater. Sci. Lett.,1993,12(1): 8-10.
[10] Reznik B, Gerthsen D, Hüttinger KJ. Carbon,2001,39(2): 215–229.