鏈�鏂板綍鐢� http://www.jim.org.cn zh-cn http://www.jim.org.cn/CN/1000-324X/current.shtml http://www.jim.org.cn 1000-324X http://www.jim.org.cn/CN/10.15541/jim20210158 http://www.jim.org.cn/CN/10.15541/jim20210142 2绾崇背鐗囷紙CeO₂ NSs锛夐�氳繃鐏劙閫�鐏敤绠�鍗曟按鐑硶鍚堟垚鐨勪腑闂翠骇鐗〤eOHCO₃绾崇背鐗囪�屽緱鍒般�傞�氳繃鎺у埗鐏劙閫�鐏椂闂�,鍙皢姘х┖浣嶅紩鍏ュ埌CeO₂绾崇背鐗囦腑銆傜粨鏋滆〃鏄�,閫�鐏�2 min寰楀埌鐨凜eO₂绾崇背鐗囷紙CeO₂-2min NSs锛夊CO姘斾綋琛ㄧ幇鍑轰紭寮傜殑閲嶅鎬у拰閫夋嫨鎬с�傚挨鍏舵槸,鍦�450 鈩冨500 μL/L CO鐨勭浉搴�/鎭㈠鏃堕棿闈炲父蹇紙2 s/2 s锛�,鍦ㄥ鑼冨洿鍐咃紙10~10000 μL/L锛塁O娴撳害涓庡搷搴斿�间箣闂村瓨鍦ㄨ壇濂界殑鍑芥暟鍏崇郴銆侰eO₂-2min NSs浼樼鐨勬皵鏁忔�ц兘鍙綊鍥犱簬澶氬瓟浜岀淮缁撴瀯楂樼殑姣旇〃闈㈢Н鍜屾櫠浣撳唴涓板瘜鐨勬哀绌轰綅銆傝繖椤瑰伐浣滃璁捐妫�娴嬪鑼冨洿姘斾綋鐨勫揩鍝嶅簲姘斾綋浼犳劅鍣ㄦ彁渚涗簡鏂规硶銆俔]> http://www.jim.org.cn/CN/10.15541/jim20210139 4)₂WS₄锛夊～鍏呰嚦纰崇鍐�,鐒跺悗鐪熺┖鐑垎瑙ｅ弽搴斿埗寰椾骇鐗┿�傞�氳繃鎷夋浖鍏夎氨銆乆灏勭嚎琛嶅皠鍜屽師瀛愬垎杈ㄩ�忓皠鐢甸暅琛ㄥ緛鍙戠幇锛氱⒊绠″唴闄愬煙鐢熼暱鐨勪富瑕佷骇鐗╀负涓�缁翠簹姘у寲鐗￤₃O₈绾崇背绾�,鍏跺吀鍨嬬嚎瀹戒负1.23~1.93 nm,瀵瑰簲4~5鍒楅挩姘у師瀛愰摼,闀垮害鍙揪鏁板崄寰背銆俉₃O₈绾崇背绾夸笌纰崇鍐呭涔嬮棿涓昏涓鸿寖寰峰崕鍔涚浉浜掍綔鐢紙闂磋窛绾�0.35 nm锛�,涓哄垎绂诲強琛ㄥ緛W₃O₈绾崇背绾跨殑鏈緛鐗规�ф彁渚涗簡鏂逛究,璇ユ柟娉曚篃鏈夋湜搴旂敤浜庡悎鎴愬叾浠栦簹鍖栧璁￠噺姣旂殑涓�缁磋繃娓￠噾灞炴哀鍖栫墿绾崇背绾裤�俔]> http://www.jim.org.cn/CN/10.15541/jim202100125 http://www.jim.org.cn/CN/10.15541/jim20210109 http://www.jim.org.cn/CN/10.15541/jim20210076 2澶嶅悎鏉愭枡浣滀负鍙鍏夊偓鍖栧墏鐢ㄤ簬姹℃煋鐗╅檷瑙ｃ�傜粨鏋滆〃鏄�,澶嶅悎鏉愭枡涓瑿Ds銆丆u²⁺涓嶵iO₂绱у瘑缁撳悎鍦ㄤ竴璧�,鍙鍏夊尯鍚告敹鏄庢樉澧炲己,鑽у厜鍙戝皠鏁堢巼闄嶄綆銆侰Ds涓嶤u²⁺鐨勫紩鍏ヤ骇鐢熷崗鍚屾晥搴�,浣垮鍚堟潗鏂欑殑绂佸甫瀹藉害闄嶄綆鍒�2.35eV,骞舵湁鏁堟姂鍒朵簡鐢靛瓙-绌虹┐鐨勫鍚堛�備互缃椾腹鏄嶣涓烘薄鏌撶墿妯″瀷鐨勫厜鍌寲鎬ц兘瀹為獙鏄剧ず,娴疯椈鍩篊Ds-Cu-TiO₂澶嶅悎鏉愭枡鍦ㄥ彲瑙佸厜鐓у皠涓嬮檷瑙hB鐨勪竴绾у弽搴旈�熺巼甯告暟鑳藉杈惧埌绾疶iO₂绾崇背棰楃矑鐨� 6.4鍊�,150 min闄嶈В鐜囨帴杩�100%,鏄疶iO₂绾崇背棰楃矑鐨�2鍊嶃�俔]> http://www.jim.org.cn/CN/10.15541/jim20200682 2鍓嶉┍浣撶殑澶氶噸閰嶄綅鍙嶅簲,鍒跺浜�3D澶氱骇瀛攔GO/TiO₂(PS)澶嶅悎鏉愭枡銆傞�氳繃涓嶅悓鎵嬫瀵规牱鍝佺殑缁撴瀯鍜屽舰璨岃繘琛岃〃寰�,鐮旂┒浜哖S娣诲姞閲忓rGO/TiO₂澶嶅悎鏉愭枡鏅朵綋缁撴瀯銆佸井瑙傚舰璨屽強鍏夊偓鍖栨�ц兘鐨勫奖鍝嶃�傚垎鍒湪妯℃嫙绱鍏夊拰鍙鍏変笅,浠ョ洂閰稿洓鐜礌(TTCH)涓虹洰鏍囨薄鏌撶墿瀵逛笉鍚孭S鍔犲叆閲忓埗澶囩殑3D澶氱骇瀛攔GO/TiO₂(PS)澶嶅悎鏉愭枡鐨勫厜鍌寲鎬ц兘杩涜璇勪环,骞跺湪妯℃嫙鍙鍏変笅,瀵�3D澶氱骇瀛攔GO/TiO₂(5wt%PS)澶嶅悎鏉愭枡杩涜浜嗗娆″惊鐜洖鏀舵祴璇曘�傜粨鏋滆〃鏄庯細rGO/TiO₂(PS)澶嶅悎鏉愭枡鍏锋湁3D澶氱骇瀛斿潡浣撶粨鏋�,GO浣滀负鍩轰綋鐨勫寮虹浉閫氳繃Ti-O-C閿繚鎸佸绾у瓟鍒氭�ч鏋剁粨鏋勭殑绋冲畾銆傚紩鍏S澧炲ぇ浜唕GO/TiO₂(PS)澶嶅悎鏉愭枡鐨勬瘮琛ㄩ潰绉�,3D澶氱骇瀛攔GO/TiO₂(7wt%PS)澶嶅悎鏉愭枡瀵筎TCH鍚搁檮鏁堢巼鏈�楂�,鑰�3D澶氱骇瀛攔GO/TiO₂(5wt%PS)澶嶅悎鏉愭枡鍏夊偓鍖栨椿鎬у拰绋冲畾鎬ф渶楂�,涓旂粡杩�4娆″惊鐜洖鏀舵祴璇�,鍏跺厜鍌寲鏁堢巼浠嶈揪81.02%;妯℃澘鍓侾S鐨勬渶浣冲紩鍏ラ噺涓�5wt%銆俔]> http://www.jim.org.cn/CN/10.15541/jim20210044 2鐨勫ぇ閲忔帓鏀�,浜虹被闈复鐨勮兘婧愬嵄鏈哄拰娓╁鏁堝簲闂鏃ョ泭涓ュ郴,鑰岄搧鍩哄偓鍖栧墏鍌寲CO₂鍔犳阿鐩存帴鍚堟垚鐑儍鏄疄鐜癈O₂鍑忔帓鍙奀O₂杞寲涓庡埄鐢ㄧ殑鏈�浣抽�斿緞涔嬩竴銆傛湰鐮旂┒閲囩敤娴告笉娉曞埗澶囦簡姘у寲閿�(ZrO₂)璐熻浇閾侀挻鍌寲鍓�(Fe-Co/ZrO₂)鍜孼rO₂璐熻浇閾侀挻閽惧偓鍖栧墏(Fe-Co-K/ZrO₂)鐢ㄤ簬鍌寲CO₂鍔犳阿鍒朵綆纰崇儻鐑�(C₂⁼-C₄⁼),閲嶇偣鑰冨療浜咾鍚噺瀵瑰偓鍖栧弽搴旀椿鎬х殑褰卞搷銆傛椿鎬ф祴璇曠粨鏋滆〃鏄�,鍦�300 鈩冨拰1.5 MPa涓�,鍔犲叆K浣緾O₂杞寲鐜囩敱40.8%鎻愰珮鍒�44.8%,浣庣⒊鐑儍閫夋嫨鎬т粠0.23%澧炶嚦68.5%,骞舵彁楂樹簡鍙嶅簲鎬ц兘鐨勭ǔ瀹氭�с�傝〃寰佺粨鏋滄樉绀�,鍔犲叆K浣縁e鐗╃鐨勫灞傜數瀛愬瘑搴﹀澶�,鎻愰珮浜咶e瀵笴O₂鐨勫惛闄勫己搴�,淇冭繘浜嗙⒊鍖栭搧鐨勫舰鎴�,骞舵湁鍒╀簬CO₂鍦‵e鐗╃涓婂惛闄勫悗鍙戠敓鐩存帴瑙ｇ,鎻愬崌浜咰O₂鍔犳阿鍒朵綆纰崇儻鐑冩�ц兘銆俔]> http://www.jim.org.cn/CN/10.15541/jim20210105 -1 (200 mA·g^-1),棣栧懆搴撲粦鏁堢巼涓�69.2%;鍦�800 mA·g^-1寰幆330鍛ㄥ悗,瀹归噺淇濇寔鐜囦粛鍙揪88%,灞曠幇鍑轰簡浼樺紓鐨勫偍閽犲惊鐜�ц兘銆傝繖寰楃泭浜庢満姊拌緟鍔╁寲瀛﹀悎閲戝寲/閰告憾瑙ｅ幓鍚堥噾鍖栧鍟嗗搧鍖朣b鐨�“棰勭矇鍖�”浣滅敤,淇冭繘浜嗘潗鏂欑殑绾崇背鍖栧拰澶氬瓟鍖�,缂撹В浜嗗厖鏀剧數杩囩▼涓殑浣撶Н鑶ㄨ儉,瀹炵幇浜嗛珮鐨勫惊鐜ǔ瀹氭�с�傝繖绉嶅父娓╁悎閲戝寲/鍘诲悎閲戝寲鐨勬柟娉曚负鍒跺寰幆绋冲畾鐨勫偍閽犲悎閲戣礋鏋佹潗鏂欐彁渚涗簡鏂扮殑閫斿緞銆俔]> http://www.jim.org.cn/CN/10.15541/jim20210091 f/SiC)锛屽苟鐮旂┒浜嗗瓟闅欑粨鏋勫鐔斾綋娴告鼎鍜屽埗澶嘢iC_f/SiC澶嶅悎鏉愭枡鐨勫奖鍝嶃�傜爺绌剁粨鏋滆〃鏄庯紝鍏锋湁杈冨潎鍖�瀛斿緞鐨勯鍒朵綋鍙互浣跨啍浣撴蹈娑︽洿鍏呭垎锛屼笖鍏锋湁鏇村皯鐨勬畫浣欏瓟闅欏強杈冮珮鐨勫鍚堟潗鏂欏姏瀛︽�ц兘銆傝鐮旂┒瀵癸紵鍙嶅簲鐔旀笚鍒跺SiC鍩哄鍚堟潗鏂欑殑瀛旂粨鏋勮皟鎺у叿鏈夋寚瀵兼剰涔夈�俔]> http://www.jim.org.cn/CN/10.15541/jim20200703 http://www.jim.org.cn/CN/10.15541/jim20210070 2)浣滀负涓�绉嶈繃娓￠噾灞炴哀鍖栫墿,鑳藉鍝嶅簲澶栫晫娓╁害鍙樺寲骞跺彂鐢熷崐瀵间綋-閲戝睘鐩稿彉,鐩稿彉杩囩▼涓即闅忕潃绾㈠娉㈡閫忚繃鐜囩殑澶у箙搴︽敼鍙�,鍦ㄦ櫤鑳界獥棰嗗煙鍙楀埌骞挎硾鍏虫敞銆傝繎骞存潵,鍏充簬VO₂鍒跺鏂瑰紡銆佺浉鍙樻満鐞嗕互鍙婃敼鍠勮皟鍏夎兘鍔涚瓑鏂归潰鐨勭爺绌堕涓轰赴瀵屻�傜劧鑰�,鍦ㄥ疄闄呭簲鐢ㄤ腑浠嶉潰涓寸潃鎶�鏈摱棰堝拰鎸戞垬,濡傛湰寰佺浉鍙樻俯搴﹁緝楂樸�佸彲瑙佸厜閫忚繃鐜囪緝浣庛�佸お闃宠兘璋冭妭鏁堢巼涓嶈冻銆佽�愬�欑ǔ瀹氭�ц緝宸�侀鑹茶垝閫傚害杈冧綆(鍛堢幇妫曢粍鑹�)绛夈�傜洰鍓�,VO₂鏈韩鎬ц兘鏀瑰杽鐨勭浉鍏崇爺绌跺凡鏈夊緢澶�,鎻愬崌鍏舵�ц兘鐨勯�氱敤鎵嬫濡傚厓绱犳幒鏉傘�佸灞傝啘缁撴瀯璁捐銆佸井缁撴瀯璁捐绛夊凡琚箍娉涢噰鐢ㄣ�傛湰鏂囨�荤粨浜哣O₂閫氱敤鎬ц兘鐨勬彁鍗囩瓥鐣�,鐫�閲嶄粙缁嶄簡VO₂鍩烘櫤鑳界獥鍦ㄥ疄闄呭簲鐢ㄤ腑鏈嶅焦鎬ц兘銆佷綆娓╂煍鎬у埗澶囦互鍙婇鑹茶皟鎺х瓑鏂归潰鐨勬渶鏂扮爺绌惰繘灞�,鍚屾椂浠庣毊鑲よ垝閫傛�у拰鐜鍙嬪ソ鎬х瓑鏂归潰鍒嗘瀽鍜屽睍鏈涗簡鏈潵鐨勫彂灞曠瓥鐣ャ�俔]> http://www.jim.org.cn/CN/10.15541/jim20210063 2 g^-1,瀛斿涓�0.673 cm³ g^-1銆俍eta鐢典綅鍒嗘瀽琛ㄦ槑,璇ュ井鐞冨湪pH=3-10鑼冨洿鍐呬繚鎸佽〃闈㈢數璐熸�с�傚皢纭呴吀闀嶅井鐞冪敤浜庡鐞嗙⒈鎬у搧绾㈡憾娑�,鍚搁檮杩囩▼绗﹀悎鍑嗕簩绾у姩鍔涘妯″瀷銆傚湪鍒濆娴撳害涓�50 mg·L^-1鐨勬潯浠朵笅,鍚搁檮瀹归噺鍙揪120.7 mg·g^-1,鑴遍櫎鐜囦负96.6%,杩滀紭浜庢敼鎬х矘鍦熷強杩戝勾鏉ユ姤閬撶殑澶氱鏉愭枡銆傚惛闄勯噺涓庡钩琛℃祿搴︾殑鏁版嵁琛ㄦ槑,纰辨�у搧绾㈠湪纭呴吀闀嶅井鐞冧笂鐨勫惛闄勭鍚團reundlich鍚搁檮妯″瀷,1/n=0.1678,琛ㄦ槑璇ュ惛闄勪负澶氬眰闈炲潎鐩稿惛闄勪笖鍚搁檮浣滅敤鍔涘己銆俔]> http://www.jim.org.cn/CN/10.15541/jim202100056 3^2-锛夊凡琚瘉瀹炲叿鏈変績杩涙垚琛�绠℃�ц兘,浣嗗叾鏈夋晥娲绘�х瀛愭祿搴﹁寖鍥存瘮杈冪獎,浠呭湪0.79~1.8 μg/mL涔嬮棿銆傚洜姝ょ簿纭帶鍒剁粍缁囧伐绋嬫潗鏂欑殑绂诲瓙閲婃斁娴撳害,浣挎潗鏂欓噴鏀剧殑绂诲瓙鑳借緝闀挎椂闂翠繚鎸佸湪鏈夋晥娲绘�ф祿搴﹁寖鍥�,瀵逛簬缁勭粐宸ョ▼搴旂敤鍏锋湁閲嶈鎰忎箟銆傛湰鐮旂┒閫氳繃璋冭妭鐢电汉涓濆瓟寰勫ぇ灏忓強纭呴吀閽欑撼绫崇嚎鐨勪笉鍚屽鍚堟柟寮�,鍒跺浜嗗绉嶇閰搁挋澶嶅悎鐢电汉涓濈氦缁存敮鏋�,骞舵瘮杈冧簡鍏跺湪浣撳鐜涓嬬殑绂诲瓙閲婃斁妯″紡鍙婂浜鸿剱闈欒剦鍐呯毊缁嗚優鐨勫娈栦績杩涗綔鐢ㄣ�傚疄楠岀粨鏋滆〃鏄�,娣风汉鍙婂悓鏃剁數鍠�-鐢电汉澶嶅悎鏂瑰紡鐨勫皬瀛斿緞纭呴吀閽欏鍚堢數绾烘敮鏋剁敱浜庨珮鍒嗗瓙鐨勭枏姘翠綔鐢ㄥ拰灏忓瓟寰勭粨鏋勫绂诲瓙鎵╂暎鐨勯樆纰�,鍙互瀹炵幇绂诲瓙缂撻噴銆傞�氳繃浣撳缁嗚優瀹為獙鍙戠幇,鍏锋湁绂诲瓙缂撻噴鏁堟灉鐨勬敮鏋跺彲浠ユ洿濂藉湴淇冭繘浜鸿剱闈欒剦鍐呯毊缁嗚優鐨勫娈�,璇存槑閫氳繃璋冩帶鏀灦绂诲瓙缂撻噴,鍙互鏈夋晥璋冩帶鍏剁敓鐗╂椿鎬�,鑾峰緱鏈�浣崇粍缁囧伐绋嬪簲鐢ㄦ晥鏋溿�俔]> http://www.jim.org.cn/CN/10.15541/jim20210043 http://www.jim.org.cn/CN/10.15541/jim202100034 2O₄閫忔槑闄剁摲鐨勯珮娓╂柇瑁傚己搴﹀拰鏂闊ф��,鍏堕娴嬬粨鏋滀笌瀹為獙鍊煎惢鍚堣壇濂姐�傜爺绌惰〃鏄�,MgAl₂O₄涓槼绂诲瓙鍙嶄綅鐜囥�佸寲瀛﹂敭纭害鍜屼綋妯￠噺闅忔俯搴︾殑鍙樺寲鍦�800鈩冨墠鍚庡瓨鍦ㄦ樉钁楀樊寮�,鐒惰�岀敱浜庨厤浣嶅闈綋鐨勮�﹀悎浣滅敤,闃崇瀛愬弽浣嶇殑娓╁害鏁堝簲涓嶄細鏄捐憲褰卞搷MgAl₂O₄閫忔槑闄剁摲鐨勯珮娓╃儹鏈烘鎬ц兘銆俔]> http://www.jim.org.cn/CN/10.15541/jim20210013 2鐩歌浆鍙樹负m-ZrO₂鐩革紝浠庨《閮ㄨ嚦搴曢儴鐩稿彉绋嬪害渚濇鍑忓急銆傜爺绌惰繕鍙戠幇锛岀敱浜庣啍铻嶇殑CMAS鏇存槗娌跨潃娑傚眰鐨勬櫠鐣岃繘琛屾笚閫忓拰渚佃殌锛孋MAS璇卞鐩稿彉涓昏鍙戠敓鍦ㄦ櫠鐣屽銆俔]> http://www.jim.org.cn/CN/10.15541/jim20210092 2)杩樺師鍒跺鍚堟垚姘�(CO鍜孒₂娣峰悎姘�),涓嶄粎鍙互瀹炵幇纰冲惊鐜檷浣庢俯瀹ゆ晥搴�,鑰屼笖鑳界紦瑙ｈ兘婧愬嵄鏈恒�傝�屽疄鐜癈O₂璧勬簮鍖栧埄鐢ㄧ殑鍏抽敭鍦ㄤ簬鍌寲鍓傝璁°�傛湰鐮旂┒閲囩敤閲戝睘绂诲瓙鍏辨矇娣�娉曞埗澶囦簡CuO鍙奀uO/ZnO澶嶅悎姘у寲鐗╃撼绫虫潗鏂�,閫氳繃璋冭妭鍌寲鍓傜粍鍒�,鎺㈢┒鍏跺湪涓嶅悓鐢靛娍涓嬬數鍖栧CO₂杩樺師鍒跺鍚堟垚姘旂殑鎬ц兘銆傜粨鏋滆〃鏄庯細寮曞叆閿�(Zn)鐗╃鍙互鍑忓急涓棿鐗〤O₂^•?鍦ㄥ偓鍖栧墏涓婄殑鍚搁檮寮哄害,瀵艰嚧CO鐨勬硶鎷夌鏁堢巼(FE)闄嶄綆,姘㈡皵FE澧炲姞,浠庤�屽疄鐜颁笉鍚岀數鍔夸笅鍚堟垚姘擟O/H₂鍦�1/1~1/4鑼冨洿鍐呯殑鍙帶璋冭妭銆傚挨鍏舵槸,褰撳墠椹辨恫涓摐鍜岄攲閰嶆瘮涓�1 : 2鏃�,鍦�-0.9 V(vs.RHE)鐨勭數鍔夸笅,CO鍜孒₂鎬�FE鍙珮杈�84%銆俔]> http://www.jim.org.cn/CN/10.15541/jim20210090 +_VB),涓旂緹鍩鸿嚜鐢卞熀(•OH)銆佸崟绾挎�佹哀(¹O₂)銆佽秴姘ц嚜鐢卞熀(•O₂-)銆佺～閰告牴鑷敱鍩�(SO₄^-•)涔熷弬涓庝簡闄嶈В鍙嶅簲銆傛渶鍚�,鏈枃鍒濇闃愭槑浜咰o-doped CuO鍗忓悓鍙鍏夋椿鍖朠MS闄嶈В鏈夋満姹℃煋鐗╃殑鍙嶅簲鏈虹悊銆俔]> http://www.jim.org.cn/CN/10.15541/jim20210080 http://www.jim.org.cn/CN/10.15541/jim202100078 http://www.jim.org.cn/CN/10.15541/jim20200751 3绾崇背鐗囩殑鍒跺鍙婂叾澶氬姛鑳藉厜瀛︽不鐤楁�ц兘銆傞噰鐢ㄩ珮娓╁浐鐩告硶鍚堟垚FePS₃鍧椾綋骞堕�氳繃瓒呭０鍗忓姪鐨勬恫鐩稿墺绂绘硶寰楀埌FePS₃绾崇背鐗�,璇ョ撼绫崇墖鐨勫钩鍧囨按鍚堢矑寰勫皬浜�200 nm锛堝钩鍧�153nm锛�,瀵�1064 nm婵�鍏夌殑鍏夌儹杞崲鏁堢巼涓�19.7%,涓旇兘鍦�660 nm婵�鍏夎緪鐓т笅浜х敓娲绘�ф哀銆傜粏鑳炲疄楠岀粨鏋滆〃鏄�,FePS₃绾崇背鐗囧叿鏈夎壇濂界殑鍏夌儹娌荤枟鍜屽厜鍔ㄥ姏瀛︽不鐤楁晥鏋溿�傚洜姝�,FePS₃绾崇背鐗囧彲鍚屾椂浣滀负鍏夌儹鍓傚拰鍏夋晱鍓傝幏寰楀厜鐑�-鍏夊姩鍔涘鑱斿悎娌荤枟鑲跨槫鍔熻兘,鍏锋湁杈冨ぇ鐨勮偪鐦ゆ不鐤楀簲鐢ㄦ綔鍔涖�俔]> http://www.jim.org.cn/CN/10.15541/jim20210032 k鍧囧�艰仛绫绘柟娉曞淇″彿杩涜浜嗗垎绫�,缁撳悎鎴潰鎵弿鐢甸暅瑙傛祴缁撴灉纭畾楂樻俯鎶楁哀鍖栨秱灞傚湪寮洸杞借嵎涓嬬殑淇″彿鍒嗗埆瀵瑰簲鍩轰綋鍙樺舰銆佽〃闈㈠瀭鐩磋绾广�佹粦鍔ㄥ瀷鐣岄潰瑁傜汗鍜屽紶寮�鍨嬬晫闈㈣绾�,閫氳繃蹇�熷倕閲屽彾鍙樻崲寰楀埌浜嗗悇绫讳俊鍙风殑涓婚鍒嗗埆涓�100銆�310銆�590鍜�450kHz,鍊熷姪灏忔尝鍒嗘瀽寰楀埌浜嗗悇淇″彿鐨勫皬娉㈣兘閲忕郴鏁般�傛秱灞傚集鏇插け鏁堣繃绋嬩富瑕佸寘鎷洓涓樁娈�,鍒嗗埆涓哄彈鎷変晶琛ㄩ潰鍨傜洿瑁傜汗钀岀敓鐨勫垵濮嬫崯浼ら樁娈点�佽〃闈㈠瀭鐩磋绾瑰娈栭樁娈点�佷袱渚х晫闈㈣绾瑰揩閫熸墿灞曠殑鎹熶激绉疮闃舵鍜屽彈鍘嬩晶娑傚眰鏄庢樉鍓ヨ惤鐨勫畯瑙傚墺钀介樁娈点�俔]> http://www.jim.org.cn/CN/10.15541/jim20210015 http://www.jim.org.cn/CN/10.15541/jim20200745 2/g,鏄庢樉楂樹簬鐩存帴鐓呯儳鍒跺鐨勭敓鐗╃⒊锛�132.7 m²/g锛夊拰纰辨敼鎬х敓鐗╃偔锛�177.2 m²/g锛夈�傝繘涓�姝ヨ瘎浠蜂簡璇ュ鍚堢墿瀵规按涓搮绂诲瓙鍚搁檮鎬ц兘,缁撴灉琛ㄦ槑鍦ㄦ按涓搮绂诲瓙娴撳害涓�120 mg/L,鑶ㄦ鼎鍦熶笌鐜夌背鑺畫娓ｈ川閲忔瘮涓�1:5,鐢ㄩ噺涓�1g/L鏉′欢涓�,鍚搁檮6h鍚庨搮绂诲瓙鍘婚櫎鐜囪揪98%,鍚搁檮閲忎负109.6 mg/g,鍧囬珮浜庣敓鐗╃偔锛�13.4 mg/g锛夈�佽啫娑﹀湡锛�72.9 mg/g锛夊拰纰辨敼鎬х敓鐗╃偔锛�86.9 mg/g锛夈�傛澶�,閲囩敤CaO-Bet-CB瀵归搮绂诲瓙姹℃煋鍦熷￥杩涜绋冲畾鍖栧鐞�,褰撳湡澹や腑閾呯瀛愭祿搴︿负2200 mg/kg,CaO-Bent-CB鐢ㄩ噺涓哄湡澹ゅ共閲嶇殑8%鏃�,鍦╬H=3.2鐨勭～閰�-纭濋吀娴告彁娑蹭腑娴稿嚭12 h,閰告蹈鍑洪搮绂诲瓙娴撳害浣庤嚦4.5 mg/L,浣庝簬鍗遍櫓搴熺墿閴村埆鏍囧噯鍊硷紙5 mg/L锛夈�備笂杩扮爺绌剁粨鏋滆〃鏄庤繖绉嶇敓鐗╃偔-鑶ㄦ鼎鍦熷叡鏀规�у鍚堢墿鍦ㄩ噸閲戝睘姹℃煋姘翠綋鍜屽湡澹や慨澶嶄腑鍏锋湁寰堝ソ鐨勫簲鐢ㄥ墠鏅�俔]> http://www.jim.org.cn/CN/10.15541/jim20200742 2銆丼iO₂銆丅aTiO₃銆乑nSnO₃銆丮oS₂銆佺煶澧ㄧ儻銆佷簩缁撮粦纾风瓑鏃犳満濉枡瀵瑰鍚堟潗鏂欑殑鎬ц兘鍧囨湁涓嶅悓绋嬪害鐨勪紭鍖�,鎵�鍒禩ENG鐨勮緭鍑哄姛鐜囧瘑搴︽渶楂樻彁鍗囦簡鏁板崄鍊嶃�傛湰鏂囩粨鍚堝浗鍐呭鐮旂┒鐜扮姸,鎸夌収濉枡瀵瑰熀浣撴潗鏂欒〃闈㈡�ц兘浠ュ強鐢靛鎬ц兘浼樺寲浣滅敤涓や釜鏂归潰杩涜闃愯堪,缁艰堪浜嗗鍚堟潗鏂欒杽鑶滃湪鎽╂摝绾崇背鍙戠數鏈轰腑鐮旂┒杩涘睍,骞跺睍鏈涗簡鏈潵澶嶅悎鏉愭枡鐢ㄤ簬鎻愰珮TENG杈撳嚭鎬ц兘鐮旂┒鐨勫彂灞曟柟鍚戙�俔]> http://www.jim.org.cn/CN/10.15541/jim20200738 1.06-_xGe_xTe(x=0,0.01,0.02,0.03,0.04)澶氭櫠鍧椾綋鏍峰搧銆傝繃閲忕殑Mn鍙互鏈夋晥鎶戝埗MnTe₂鐩哥殑浜х敓,鎻愰珮鍩轰綋鐩哥殑鐑數鎬ц兘銆傞�氳繃鎺烘潅4%Ge绮夋湯,鏉愭枡鐨勮浇娴佸瓙娴撳害鎻愰珮鍒�7.328×10¹⁸ cm^-3,鐢靛鐜囧湪873 K澧炲姞鍒�7×10³ S∙cm^-1,鍔熺巼鍥犲瓙鎻愬崌鑷�620 μW∙m^-1∙K^-2銆傚悓鏃�,閫氳繃鐐圭己闄峰寮哄０瀛愭暎灏勪娇鏉愭枡鐨勭儹瀵肩巼闄嶄綆鍒�0.62W∙m^-1∙K^-1,瀹炵幇浜嗗鏉愭枡鐢靛０杈撹繍鎬ц兘鐨勬湁鏁堣皟鎺с�侻n_1.02Ge_0.04Te鍦�873 K鑾峰緱浜�0.86鐨勭儹鐢典紭鍊�ZT,杈冪函MnTe鏉愭枡鎻愰珮浜�43%銆俔]> http://www.jim.org.cn/CN/10.15541/jim20200727 3+鐨勬幒鏉傛祿搴�,灏嗙粍瑁呭櫒浠剁殑鍙戝皠鍏夎氨鍜岃壊鍧愭爣浠庡喎鐧藉尯璋冩暣鍒版殩鐧藉尯銆備互楂樼函(≥99.99%)鍟嗕笟绮変綋α-Al₂O₃銆乊₂O₃銆丆eO₂涓哄師鏂�,閲囩敤鍥虹浉鍙嶅簲娉曞埗澶囦簡(Ce_xY_1-x)₃Al₅O₁₂ (x=0.0005銆�0.0010銆�0.0030銆�0.0050銆�0.0070鍜�0.0100)閫忔槑闄剁摲銆傞櫠鐡风礌鍧湪1750 鈩冪湡绌虹儳缁�20h(鐪熺┖搴�5.0×10^-5Pa),涔嬪悗鍦ㄩ┈寮楃倝涓��鐏�1450 鈩�×10 h銆備笉鍚屾幒鏉傛祿搴e:YAG闄剁摲(鍘氬害鍒嗗埆涓�0.2 mm銆�0.4 mm銆�1.0 mm)鍦�800 nm澶勭殑鐩寸嚎閫忚繃鐜囧潎澶т簬79%銆侰e:YAG鑽у厜闄剁摲鐨勭儹瀵肩巼闅忕潃娴嬭瘯娓╁害鍜屾幒鏉傛祿搴︾殑澧炲姞鑰岄檷浣庛�傞噰鐢ㄦ湁闄愬厓鏂规硶妯℃嫙涓嶅悓鍘氬害鐨凜e:YAG闄剁摲鍜孡ED缁勮鐨勭儹鍒嗗竷,姣旇緝浜嗕笁绉嶅皝瑁呮柟寮忕殑鐑垎甯冦�傚皢Ce:YAG鑽у厜闄剁摲涓嶭EDs/LDs澶嶅悎,鍒跺鍑鸿壊鍧愭爣鍒嗗埆涓�(0.3319,0.3827)鍜�(0.3298,0.3272)鐨勭櫧鍏�,鍙戝厜鏁堢巼鍒嗗埆涓�122.4lm/W鍜�201.5lm/W銆傚皢Ce:YAG鑽у厜闄剁摲鍜�10W銆�50W鍟嗙敤钃濆厜LED鑺墖缁勫悎鎴愮啛鐏叿,鍙敤浜庡晢涓氱敤閫斻�侰e:YAG閫忔槑闄剁摲鍦ㄥぇ鍔熺巼鐓ф槑鍜屾樉绀虹殑褰╄壊杞崲鏉愭枡搴旂敤棰嗗煙鏋佸叿娼滃姏銆俔]> http://www.jim.org.cn/CN/10.15541/jim20200698 ZT鍊煎湪鏁翠釜娓╁尯鍧囨湁鎻愰珮,骞跺湪773 K鏃跺彇寰楁渶澶у��0.5銆俔]> http://www.jim.org.cn/CN/10.15541/jim20200690 -1,纰冲寲娓╁害涓�900 鈩冩椂,鎵�鍒跺鐨勪腑瀛旂偔鎬ц兘鏈�浼�,鍏锋湁楂樺害鏈夊簭鐨勪簩缁村叚鏂瑰瓟閬撶粨鏋�,姣旇〃闈㈢Н涓�675 m²·g^-1,瀛斿涓�1 cm³·g^-1,瀛斿緞闆嗕腑鍦�3.84 nm宸﹀彸銆傝涓瓟鐐敤浜嶭i-S鐢垫睜鐨勬鏋佽浇浣撴潗鏂欒〃鐜板嚭鑹ソ鐨勭數鍖栧鎬ц兘,鍦�0.2C鐢垫祦瀵嗗害涓嬬粡300娆″惊鐜悗鏀剧數姣斿閲忓拰瀹归噺淇濇寔鐜囧垎鍒负688 mAh·g^-1鍜�67.1%,鍦�3C鐢垫祦瀵嗗害涓嬫瘮瀹归噺鍙揪556 mAh·g^-1銆俔]> http://www.jim.org.cn/CN/10.15541/jim20200679 2O₄閫忔槑闄剁摲,閲囩敤鍏辨矇娣�娉曞悎鎴愰挻鎺烘潅鐨勭函鐩搁晛閾濆皷鏅剁煶绾崇背绮変綋,骞堕�氳繃鐪熺┖鐑х粨缁撳悎鐑瓑闈欏帇鐑х粨(Hot Isostatic Pressing,HIP),鍒跺寰楀埌浜嗛珮璐ㄩ噺鐨�0.05at% Co:MgAl₂O₄閫忔槑闄剁摲,鍚屾椂绯荤粺鐮旂┒浜嗛鐑х粨娓╁害瀵笴o:MgAl₂O₄闄剁摲寰缁撴瀯鍜屽厜瀛︽�ц兘鐨勫奖鍝嶃�傞殢鐫�棰勭儳缁撴俯搴︿粠1500鈩冨崌楂樿嚦1650鈩�,Co:MgAl₂O₄闄剁摲鐨勭浉瀵瑰瘑搴︿粠95.2%澧炲姞鍒�98.5%,鑰屽綋棰勭儳娓╁害鍗囬珮鑷�1700鈩�,Co:MgAl₂O₄闄剁摲鐨勭浉瀵瑰瘑搴﹂檷浣庤嚦97.7锛呫�傜湡绌洪鐑у悗Co:MgAl₂O₄闄剁摲鐨勭浉瀵瑰瘑搴﹁緝浣�,鍥犳棰勭儳鍚庣殑Co:MgAl₂O₄闄剁摲鍧囦负涓嶉�忔槑鐨勩�傚綋棰勭儳娓╁害浠�1500鈩冨崌楂樺埌1700鈩�,Co:MgAl₂O₄闄剁摲鐨勫钩鍧囨櫠绮掑昂瀵镐粠2.3μm澧炲姞鍒�11.3μm銆傜粡杩嘓IP鍚庡鐞嗗悗,鍦�1550-1700鈩�×5h鐪熺┖棰勭儳鏉′欢涓嬬殑Co:MgAl₂O₄闄剁摲閮芥槸閫忔槑鐨�,鑰岀粡杩�1650鈩�×5h鐪熺┖棰勭儳缁撳悎1800鈩�×3h HIP鍚庡鐞嗙殑Co:MgAl₂O₄閫忔槑闄剁摲琛ㄧ幇鍑烘渶浣崇殑鍏夊璐ㄩ噺,鍦�400鍜�900 nm澶勭殑鐩寸嚎閫忚繃鐜囧垎鍒负81.4%鍜�85.9%,骞冲潎鏅剁矑灏哄涓�16.8μm銆傚湪500-700 nm鍜�1200-1600 nm娉㈤暱鑼冨洿鍐呯殑瀹藉惛鏀跺甫琛ㄦ槑Co²⁺宸叉幒鍏ュ皷鏅剁煶鏅舵牸涓�傛澶�,缁忚绠�,鏈�浣冲厜瀛﹁川閲忕殑鏍峰搧鍦�1540 nm澶勭殑鍩烘�佸惛鏀舵埅闈负6.18×10^-19 cm²,琛ㄦ槑浜咰o:MgAl₂O₄宸茬粡鎴愪负鍥烘�佹縺鍏夊櫒涓鍔ㄨ皟Q鍙ケ鍜屽惛鏀朵綋鐨勬渶鏈夋綔鍔涚殑鏉愭枡涔嬩竴銆俔]> http://www.jim.org.cn/CN/10.15541/jim20210030 2-6Na₂O-8K₂O-8MgO-22CaO-2P₂O₅-36B₂O₃鐨勭〖纭呴吀鐩愮敓鐗╂椿鎬х幓鐠冩蹈娉″湪SBF鐢熺悊妯℃嫙娑蹭腑,鏂藉姞0~90 mA鐨勭數娴�,鐮旂┒鐩存祦鐢靛満瀵圭〖纭呴吀鐩愮敓鐗╃幓鐠冮檷瑙ｅ強浣撳鐭垮寲鎬ц兘鐨勫奖鍝嶃�傜爺绌剁粨鏋滆〃鏄�,鏂藉姞鐢靛満涓嶄粎鍙互鎻愰珮纭肩閰哥洂鐢熺墿娲绘�х幓鐠冪殑闄嶈В鐜囧拰绂诲瓙閲婃斁閲�,鑰屼笖鏈夊埄浜庣幓鐠冪綉缁滄按瑙ｅ拰琛ㄩ潰缇熷熀鍖�,鍔犻�熺緹鍩虹７鐏扮煶鐨勭敓鎴愩�傚叾涓け閲嶇巼姣斿鐓х粍鎻愰珮浜�3%~5%,纭煎拰閽欑殑绂诲瓙閲婃斁閲忓垎鍒緝瀵圭収缁勬彁楂樹簡2.3~2.9鍊嶅拰1.9-2.3鍊嶃�傚纭肩閰哥洂鐢熺墿娲绘�х幓鐠冭〃闈㈢粨鏋勫垎鏋愬緱鍑�,鏆撮湶鍦ㄧ數鍦轰笅鐨勬牱鍝佽〃闈㈢敓鎴愪簡纾风伆鐭冲眰銆傚簲鐢ㄧ洿娴佺數鍦哄彲浠ユ彁楂樼敓鐗╂椿鎬х幓鐠冪殑闄嶈В鍙婁綋澶栫熆鍖栨�ц兘,涓烘彁鍗囬淇鏁堟灉鎻愪緵浜嗕竴绉嶆柊鎬濊矾銆俔]> http://www.jim.org.cn/CN/10.15541/jim20200663 4^2藟銆丯O₃^藟銆丯a⁺銆丮g⁺绛夊共鎵扮瀛愬叡瀛樼殑鐜涓嬩娇鐢ㄣ�傛澶栵紝寰楃泭浜庨摐璐熻浇鍑瑰嚫妫掔煶缁撴瀯鍐咃紝璇ュ鍚堟潗鏂欏睍鐜板嚭杈冨己鐨勬姉姘у寲鎬ц兘锛屼笖鍚搁檮鍚庝骇鐗╀篃鍏锋湁杈冨己鐨勭ǔ瀹氭�с�俔]> http://www.jim.org.cn/CN/10.15541/jim20200653 2S鍥犲叿鏈変紭寮傜殑鐗╃悊鍖栧鎬ц兘,鍦ㄥ偓鍖栥�佷紶鎰熷強鍏夌數瀛愮瓑棰嗗煙鍏锋湁骞块様鐨勫簲鐢ㄧ┖闂淬�傛湰宸ヤ綔鍒╃敤涓�绉嶅尯鐔旀妧鏈埗澶囦簡灏哄涓�Ø18mm× 50 mm鐨凙g₂S骞跺鍏舵綔鍦ㄧ儹鐢垫�ц兘杩涜浜嗙爺绌躲�侫g₂S鍦�450 K娓╁害浠ヤ笅鍏锋湁鏍囧噯鐨�α-Ag₂S鍗曟枩P2₁/c缁撴瀯,450 K浠ヤ笂鍙戠敓鐩稿彉鎴愪负绔嬫柟β-Ag₂S鐩搞�侫g₂S鍦�300~650 K鑼冨洿濮嬬粓鍏锋湁璐熺殑Seebeck绯绘暟鑰屽憟鐜�n鍨嬪崐瀵间綋鐗瑰緛,杩欎富瑕佹槸鍥犱负鏉愭枡涓瓨鍦ˋg闂撮殭绂诲瓙鑰屾彁渚涗簡澶氫綑鐢靛瓙銆侫g₂S鐨凷eebeck绯绘暟鍦ㄥ娓╀笅绾︿负-1200 µV·K^-1,440 K鏃堕檷涓�-680 µV·K^-1,褰撹浆鍙樹负β-Ag₂S鍚庡垯澶у箙闄嶈嚦~-100 µV·K^-1銆�α-Ag₂S鐨勭數瀵肩巼鍑犱箮涓洪浂,鐒惰�屽湪鍒氬彂鐢�β-Ag₂S鐩稿彉鏃�,鐢靛鐜囩獊鐒跺鍔犺嚦~40000.5 S·m^-1,鑰屽悗闅忕潃娓╁害鎸佺画鍗囬珮,鍏跺�煎湪650 K闄嶄綆涓�33256.2 S·m^-1銆傞湇灏旀祴璇曡〃鏄嶢g₂S鐨勮浇娴佸瓙娴撳害n_H鍦ㄧ浉鍙樻椂鍙粠~10¹⁷ cm^-3鍓х儓澧炲姞鍒皛10¹⁸ cm^-3閲忕骇銆�α-Ag₂S鍜�β-Ag₂S鐨勬�荤儹瀵肩巼κ鍑犱箮鏄父鏁�,鍒嗗埆涓簙0.20 W·m^-1·K^-1鍜寏0.45 W·m^-1·K^-1銆傛渶缁圓g₂S鍦�580 K鑾峰緱鏈�澶�ZT鍊�0.57,璇存槑瀹冩槸涓�绉嶅緢鏈夊彂灞曟綔鍔涚殑涓俯鐑數鏉愭枡銆俔]> http://www.jim.org.cn/CN/10.15541/jim20200623 T_C≈22-3 K)涓�,闄や簡4f鐢靛瓙婊″３灞傜殑LuB₁₂涔嬪,鍏朵粬绋�鍦�-纭煎崄浜屽寲鍚堢墿(绠�绉癛B₁₂,R涓虹█鍦熷厓绱燭b, Dy, Ho, Er, 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2/NiO澶嶅悎鍗婂浣撶撼绫崇氦缁淬�傞噰鐢ㄦ壂鎻忕數瀛愭樉寰暅(SEM),X灏勭嚎琛嶅皠浠�(XRD)鍜岃兘閲忚壊鏁灏勭嚎鍏夎氨浠�(EDS)瀵规牱鍝佺殑褰㈣矊,缁撴瀯浠ュ強鍚勫厓绱犲惈閲忚繘琛岃〃寰併�備互涔欓唶涓虹洰鏍囨皵浣�,鎺㈢┒SnO₂/NiO绾崇背绾ょ淮鐨勬皵浣撲紶鎰熸�ц川,浠ュ強Sn鍚噺瀵瑰鍚堢撼绫崇氦缁存皵鏁忔�ц兘鐨勫奖鍝嶃�傜爺绌剁粨鏋滆〃鏄�,SnO₂/NiO澶嶅悎绾崇背绾ょ淮鍏蜂笁缁寸綉鐘剁粨鏋�,SnO₂澶嶅悎瀵筃iO绾崇背绾ょ淮鐨勬皵鏁忔�ц兘鍏锋湁鏄庢樉鐨勫寮轰綔鐢ㄣ�傞殢鐫�SnO₂鍚噺鐨勫鍔�,澶嶅悎绾ょ淮瀵逛箼閱囨皵浣撶殑鍝嶅簲鐏垫晱搴﹀寮�,鍏朵腑鍝嶅簲鏈�楂樼殑澶嶅悎绾崇背绾ょ淮鍦ㄦ渶浣冲伐浣滄俯搴�160鈩冩潯浠朵笅瀵逛綋绉垎鏁颁负100×10^-6涔欓唶姘斾綋鐨勫搷搴旂伒鏁忓害涓�13.4,鏄疦iO绾崇背绾ょ淮鏈�澶у搷搴旂伒鏁忓害鐨�8.38鍊嶃�備笌甯傞潰甯歌鐨勪箼閱囨皵浣撲紶鎰熷櫒MQ-3鐩告瘮,SnO₂/NiO澶嶅悎绾崇背绾ょ淮鐨勬渶浣冲伐浣滄俯搴︽洿浣�,鍚屾椂鍏锋湁鏇撮珮鐨勫搷搴旂伒鏁忓害,鍏锋湁涓�瀹氱殑瀹為檯搴旂敤浠峰�笺�俔]> http://www.jim.org.cn/CN/10.15541/jim20200664 3^2-銆丼eO₃^2-/PO₄^3-锛夊樊寮傚鑷翠綆鎺烘潅鐜囥�傛湰鐮旂┒鎻ず浜嗘幒鏉傝涓轰笌绂诲瓙鐗规�т箣闂寸殑鍚堢悊鑱旂郴,涓哄姛鑳藉寲缇熷熀纾风伆鐭崇殑璁捐鍜屽紑鍙戞彁渚涙湁鐩婄殑鍙傝�冨熀纭�銆俔]> http://www.jim.org.cn/CN/10.15541/jim20200635 2Se₃缁勫厓浠ヨ皟鎺鍨婸bTe鍩轰綋鐨勭儹銆佺數浼犺緭鎬ц兘銆傜爺绌跺彂鐜�, PbS涓嶴b₂Se₃缁勫厓鍙垎鍒彁鍗囧姛鐜囧洜瀛愩�侀檷浣庣儹瀵肩巼銆傞�氳繃鎵╁ぇ甯﹂殭銆佸鍔犵偣缂洪櫡銆佺浜岀浉寮ユ暎绛夐�斿緞鍙敼鍠勮兘甯︺�佸姞鍓ф暎灏�, 浠庤�屾湁鏁堟彁鍗囩儹鐢典紭鍊�ZT銆傚叾涓�(PbTe)_0.94(PbS)_0.05(Sb₂Se₃)_0.01琛ㄧ幇鍑烘渶浣崇殑鐑數鎬ц兘,700 K鏃�ZT鏈�澶у�间负1.7,涓�ZT骞冲潎鍊艰緝PbTe鍩轰綋鏄捐憲鎻愰珮, 杩欒〃鏄庡垎姝ュ紡鍙岀粍鍏冭皟鎺у彲涓烘敼鍠勫叾瀹冩潗鏂欎綋绯荤殑鐑數鎬ц兘鎻愪緵鎶�鏈�斿緞銆俔]> http://www.jim.org.cn/CN/10.15541/jim20200576 4Ti₅O₁₂鐢垫瀬鐗囪〃闈�,淇グ鍚庣數鏋佽〃闈㈤潪甯稿厜婊�,褰㈡垚浜嗗潎鍖�鐨勯潪鏅舵�佺７閰搁攤鍖呰灞傘�傚湪鐢靛帇鑼冨洿涓�0.01-3 V鐨勫厖鏀剧數娴嬭瘯缁撴灉鏄剧ず,璇ュ寘瑕嗗眰鍙樉钁楁敼鍠勭數鏋佺殑鍊嶇巼鎬ц兘鍜屽惊鐜�ц兘銆傚綋鍏呮斁鐢电數娴佸瘑搴﹀垎鍒负35鍜�1750 mA∙g^-1鏃�,鐢垫睜瀹归噺鍙互杈惧埌265鍜�151 mAh∙g^-1,杩滈珮浜庢湭鍖呰鐢垫睜鐨�240鍜�22 mAh∙g^-1銆傚苟浠�88 mA∙g^-1鐨勭數娴佸瘑搴﹁繘涓�姝ュ厖鏀剧數200涓惊鐜悗,浠嶄繚鐣欎簡238 mAh∙g^-1鐨勯珮鍙�嗗閲忋�傝繖鏄敱浜庨潪鏅舵�佺７閰搁攤鍖呰灞傚彲绋冲畾鐢佃В璐ㄧ晫闈�,淇濇寔绮掑瓙闂寸數瀛愰�氶亾鐨勫畬鏁存��,骞跺湪鐢垫瀬琛ㄩ潰褰㈡垚浜よ仈绂诲瓙瀵肩數缃戠粶,浣垮緱鏀规�х數鏋佺殑鍊嶇巼鎬ц兘鍜屽惊鐜ǔ瀹氭�ф樉钁楁彁楂樸�俔]> http://www.jim.org.cn/CN/10.15541/jim20200522 0.8Mn_0.2O₂浜屽厓鏉愭枡,鍐嶆幒鍏ヤ笉鍚屾瘮渚嬬殑Co銆丄l瀵规潗鏂欒繘琛屾敼鎬х爺绌躲�傜粨鏋滆〃鏄�,鏀规�у悗鐨勬潗鏂欐�ц兘鏄庢樉鏀瑰杽,鐗瑰埆鏄疞iNi_0.8Mn_0.1Co_0.08Al_0.02O₂鍦�2.75~4.35 V銆�1C涓嬪惊鐜�100娆″悗瀹归噺淇濇寔鐜囪揪鍒�91.39%,鍦�5C涓嬫斁鐢垫瘮瀹归噺浠嶆湁160.03 mAh∙g^-1,骞朵笖鎺烘潅鍚庣殑鏉愭枡鍏锋湁杈冮珮鐨勭儹绋冲畾鎬�,瀹夊叏鎬у緱鍒版彁鍗囥�傚叾浼樺紓鐨勫惊鐜繚鎸佺巼褰掑洜浜嶤o銆丄l杈冨ソ鍦版姂鍒朵簡寰幆杩囩▼涓璈2→H3鐩稿彉鐨勪笉鍙�嗘�у鏉愭枡缁撴瀯绋冲畾鎬х殑鐮村潖,浠ュ強杈冨急鐨勭數鏋佸弽搴旀瀬鍖�,浣跨數鑽疯浆绉荤數闃婚檷浣庛�俔]> http://www.jim.org.cn/CN/10.15541/jim20200512 -1,鍚搁檮鍔ㄥ姏瀛﹀彲鐢ㄦ嫙浜岀骇鍔ㄥ姏瀛︽柟绋嬫潵鎻忚堪,鍚屾椂鍚搁檮杩囩▼涓鸿嚜鍙戞斁鐑繃绋嬨�俋PS鍒嗘瀽琛ㄦ槑鍚搁檮鍓傜殑涓昏鍚搁檮鏈虹悊涓轰笌闀�/閾佽繛鎺ョ殑缇熷熀鍩哄洟鍜孒EDP涔嬮棿鐨勯厤浣撲氦鎹綔鐢ㄣ�俔]> http://www.jim.org.cn/CN/10.15541/jim20200657 2Ca₂Si₂O₇)鐢熺墿闄剁摲瀵逛汉鐗欏懆鑶滄垚绾ょ淮缁嗚優澧炴畺銆佺熆鍖栫殑褰卞搷鍙婄敤浜庣墮鍛ㄩ缁勭粐鍐嶇敓鐨勫彲鑳芥�с�傞噰鐢ㄦ憾鑳�-鍑濊兌娉曞埗澶囧悎鎴愪簡Li₂Ca₂Si₂O₇闄剁摲绮変綋銆傞�氳繃浣撳妯℃嫙浣撴恫娴告场,鍙戠幇Li₂Ca₂Si₂O₇绮変綋鍏锋湁鑹ソ鐨勭緹鍩虹７鐏扮煶鐭垮寲鑳藉姏銆傜敓鐗╁缁撴灉琛ㄦ槑锛歀i₂Ca₂Si₂O₇绮変綋鐨勬蹈鎻愭恫鍦�3.125~25 mg/mL娴撳害鑼冨洿鍐呰兘鏄捐憲淇冭繘HPLFs鐨勫娈�,浣庢祿搴�(6.25 mg/mL)鏃跺彲鏄捐憲璇卞HPLFs缁嗚優浣撳鐭垮寲(p鍡棷鍡�0.05)銆侺i₂Ca₂Si₂O₇绮変綋鍏锋湁淇冭繘浜虹墮鍛ㄨ啘鎴愮氦缁寸粏鑳炲娈栧拰鐭垮寲鑳藉姏,鍙湜浣滀负鐗欏懆楠ㄧ粍缁囧啀鐢熶慨澶嶇殑鐢熺墿娲绘�ф潗鏂欍�� Abstract: How to effectively treat periodontitis and achieve regeneration of damaged periodontal tissue has always been a challenging problem in the treatment of periodontal diseases, and mineralization is one of the key factors in the normal periodontal development and function. The aim of this study was to investigate the effects of Li₂Ca₂Si₂O₇ bioceramics on proliferation and mineralization of human periodontal ligament fibroblasts (HPLFs) and possibility of its application in periodontal tissue regeneration. Li₂Ca₂Si₂O₇ ceramic powder was synthesized by sol-gel method. It was found that Li₂Ca₂Si₂O₇ powder had good ability of hydroxyapatite mineralization by immersing in simulated body fluid. The in vitro biological results showed that Li₂Ca₂Si₂O₇ powder extract could significantly promote proliferation of HPLFs in the concentration range of 3.125~25 mg/mL, and at low concentration (6.25 mg/mL), could significantly induce mineralization of HPLFs cells (p鍡棷鍡�0.05). all these experimental results reveal that the new Li₂Ca₂Si₂O₇ powder can promote proliferation and mineralization of HPLFs, and it may be a promising bioactive material for periodontal tissue regeneration.]]> http://www.jim.org.cn/CN/10.15541/jim20200639 -3锛�,鍚屾椂鍚告按鐜囦綆鑷�0.53%銆傚悓鏃舵帰璁ㄤ簡AlN濉枡鍦ㄨ閾滄澘搴旂敤涓瓨鍦ㄧ殑闂鍜岃В鍐虫柟娉�,绯荤粺鐮旂┒浜嗕笉鍚屽～鍏呮柟妗堝瑕嗛摐鏉跨粷缂樺眰鎬ц兘鐨勫奖鍝�,瀵瑰叾瀹為檯搴旂敤鍏锋湁鎸囧鎰忎箟銆俔]> http://www.jim.org.cn/CN/10.15541/jim20200624 2g^-1,鍏朵腑Fe鍏冪礌鐨勫惈閲忎负0.57wt%銆傞�氳繃鐞冨樊鐢甸暅鐩存帴瑙傚療鍒颁簡瀛ょ珛瀛樺湪鐨凢e鍗曞師瀛�,骞堕�氳繃X灏勭嚎鍚告敹绮剧粏缁撴瀯(XAFS)鍒嗘瀽纭畾Fe鍗曞師瀛愪互Fe-N₄閰嶄綅浣撳舰寮忓垎鏁ｅ湪纰冲熀鏉愭枡涓娿�侳e SA-NC鍌寲鍓傚湪0.1 mol/L KOH 婧舵恫涓崐娉㈢數浣嶄负0.85V,鏋侀檺鐢垫祦瀵嗗害涓�5.79mA cm^-2,瓒呰繃鍟嗕笟Pt/C鍌寲鍓傘�侳e SA-NC鍌寲鍓備笉浠呭ORR鍥涚數瀛愰�斿緞鏄剧ず鍑洪珮閫夋嫨鎬�(H₂O₂浜х巼鍡棷鍡�2%,杞Щ鐢靛瓙鏁颁负3.9),鍚屾椂琛ㄧ幇鍑轰紭绉�鐨勬姉鐢查唶鎬ц兘銆� Abstract: Single atom catalysts (SACs) have emerged as an attractive concept for promoting heterogeneous reactionsdue to the unique properties, such as high activity and nearly 100% atom utilization. However, the synthesis ofSACs remains a challengedue tothe sintering of metal atoms at high temperature. In this study, Fe single atom on N doped porouscarbon (Fe SA-NC)catalyst was obtained by the ultrastrong polarity of molten salt (MS). Fe SA-NC shows honeycomb-like porous morphology and possesses a high specific surface areaof 2072.5 m² g ^-1.The content of Fe element in FeSA-NC is 0.57wt%. The isolated Fe atomsare observed by AC HAADF-STEM, and the X-ray absorption fine structure (XAFS) analysis confirms that Fe atomsare dispersed in the form of Fe-N₄ on the carbonsubstrate.Fe SA-NC shows 0.85 V half-wave potential and 5.79mA cm^-2maximum current density for ORR in 0.1 mol/L KOH solution. Fe SA-NCdemonstrates highselectivityforORR four electron pathway (H₂O₂ yield 鍡棷鍡�2%, electron transfer number is 3.9), outstanding stability, and good methanol tolerance.]]> http://www.jim.org.cn/CN/10.15541/jim20200582 http://www.jim.org.cn/CN/10.15541/jim20200632 2/g,鎬诲瓟瀹逛负3.164cm³/g,鏄庢樉浼樹簬鍟嗙敤娲绘�х偔锛圷P-80,姣旇〃闈㈢Н涓�1310m²/g,鎬诲瓟瀹逛负0.816cm³/g锛夈�傚叿鏈夋渶楂樻瘮琛ㄩ潰绉殑绋诲３娲绘�х偔瀵逛簹鐢插熀钃濈殑鏈�澶у惛闄勯噺杈惧埌983mg/g,鍑犱箮鏄痀P-80锛�525mg/g锛夌殑涓ゅ�嶃�傞�氳繃鍚搁檮鍔ㄥ姏瀛︽嫙鍚�,鍚搁檮浜氱敳鍩鸿摑鐨勮繃绋嬩笌鎷熶簩绾фā鍨嬩竴鑷�,琛ㄦ槑璇ヨ繃绋嬩负鍖栧鍚搁檮銆俔]> http://www.jim.org.cn/CN/10.15541/jim20200621 http://www.jim.org.cn/CN/10.15541/jim20200555 http://www.jim.org.cn/CN/10.15541/jim20200525 +鐨勫揩閫熶紶杈�,涔熸湁瓒冲鐨勭┖闅欑紦瑙ｅ湪鑴�-宓岄攤杩囩▼涓彂鐢熺殑浣撶Н鍙樺寲銆傚緱鐩婁簬涓夌淮缁撴瀯涓ぇ閲忕殑瀛旈殭鍜岄珮寮哄害鐨勫閮ㄧ⒊灞�,澶氬瓟3D-bio-Si/C鍒跺鐨勭數鏋佽〃鐜板嚭浼樺紓鐨勭數鍖栧鎬ц兘銆傚綋鐢垫祦瀵嗗害涓�1 A/g鏃�,澶氬瓟3D-bio-Si/C鐨勫彲閫嗗閲忎负1243.2 mAh/g,寰幆400娆″悗浠嶅彲淇濇寔933.4 mAh/g,瀹归噺淇濇寔鐜囬珮杈�89%銆傚埄鐢ㄦ邯鏈ㄨ醇浣滀负鐢熺墿璐ㄧ婧愬埗澶囬珮鎬ц兘纭呭熀璐熸瀬鏉愭枡,瀹炵幇浜嗕綆鎴愭湰銆佸彲瑙勬ā鍖栥�佺豢鑹插拰鍙寔缁殑鍚堟垚璺嚎,鏈夋湜涓篠i鍩洪攤绂诲瓙鐢垫睜璐熸瀬鏉愭枡鐨勫晢涓氬簲鐢ㄦ墦涓嬪熀纭�銆俔]> http://www.jim.org.cn/CN/10.15541/jim20200507 1/2,浣嶄簬锛�110锛炴櫠鍚�,纭畾锛�110锛炴櫠鍚戞槸瑁傜汗鏈�瀹规槗鎵╁睍鐨勬櫠鍚戙�俔]> http://www.jim.org.cn/CN/10.15541/jim20200437 2MoO₆澶嶅悎鍌寲鍓傦紙Fe(III)/rGO/Bi₂MoO₆锛�,閫氳繃澶栧姞H₂O₂鏋勫缓浜嗗厜鍌寲-鑺】鍗忓悓浣撶郴,鍙鍏夌収灏�3h鍚庡彲鍏ㄩ儴闄嶈В鑻厷,鍗忓悓闄嶈В鏁堢巼鍒嗗埆鏄崟绾厜鍌寲鎴栬姮椤垮弽搴旂殑5.56鍊嶅拰2.08鍊嶃�傝繖涓昏鏄�氳繃Fe寰楀け鐢靛瓙瀹炵幇浠锋�佺殑杞彉,骞朵互姝や綔涓烘ˉ姊佸疄鐜板厜鍌寲-鑺】鐨勫崗鍚屼綔鐢ㄣ�傚悓鏃剁煶澧ㄧ儻鐨勪紭寮傚鐢垫�ц兘涓嶄粎鍏嬫湇浜嗗厜鍌寲涓厜鐢熺數瀛愮┖绌撮毦浠ュ垎绂荤殑闂,鑰屼笖淇冭繘浜咶e³⁺/Fe²⁺鐨勫惊鐜弽搴�,淇冧娇鑺】鍙嶅簲浜х敓鏇村鐨勭緹鍩鸿嚜鐢卞熀(·OH),杩涗竴姝ユ彁楂樹簡鑻厷鐨勯檷瑙ｆ晥鐜囥�傚疄楠岃�冨療浜咶e(III)鍚噺銆佸偓鍖栧墏鎶曞姞閲忋�丠₂O₂鍚噺浠ュ強pH绛夊洜绱犲鍗忓悓闄嶈В鏁堟灉鐨勫奖鍝嶃�傛番鐏疄楠岃瘉鏄�·OH鏄崗鍚岄檷瑙ｄ綋绯讳腑鏈�涓昏鐨勬椿鎬х墿绉�,鍚屾椂·O₂^-鍜宧⁺瀵归檷瑙ｆ椿鎬т篃浼氫骇鐢熶竴瀹氱殑褰卞搷,缁撳悎瀹為獙缁撴灉鎻愬嚭浜咶e(III)/rGO/Bi₂MoO₆鍏夊偓鍖�-鑺】鍗忓悓闄嶈В鑻厷鐨勬満鐞嗐�俔]> http://www.jim.org.cn/CN/10.15541/jim20200033 -1 KOH鐢佃В娑蹭腑,鐢垫祦瀵嗗害涓�1 A·g^-1鏃�,鏈幒鏉傜⒊绾崇背绠＄殑姣旂數瀹逛负62.2 F·g^-1,姘幒鏉備箣鍚庣⒊绾崇背绠＄殑姣旂數瀹逛负97.0 F·g^-1,姘�/纭叡鎺烘潅鐨勭⒊绾崇背绠℃瘮鐢靛涓�172.0 F·g^-1,姘�/纭叡鎺烘潅鍚庣⒊绾崇背绠＄殑鐢靛寲瀛︽�ц兘姣旀湭鎺烘潅鐨勬彁楂樿繎3鍊�;寰幆1000娆＄數瀹逛繚鎸佺巼杈�89%,璇存槑鎺�/纭叡鎺烘潅纰崇撼绫崇鍏锋湁鑹ソ鐨勭數鍖栧鎬ц兘銆傛澶�,缁勮鐨勫绉板瀷瓒呯骇鐢靛鍣ㄥ悓鏍峰睍绀轰簡鑹ソ鐨勭數瀹规�ц兘銆俔]> http://www.jim.org.cn/CN/10.15541/jim20200540 2钖勮啘涓昏閫氳繃鏈烘鍓ョ娉曞拰姘旂浉娌夌Н娉曞埗寰�,鏈爺绌堕噰鐢ㄤ竴绉嶇畝鍗曟湁鏁堢殑鍙湪SiO₂/Si琛簳涓婂埗澶嘝dSe₂钖勮啘鐨勬柟娉曘�傞�氳繃楂樼湡绌虹鎺ф簠灏勬妧鏈湪SiO₂/Si琛簳涓婃矇绉竴灞侾d閲戝睘钖勮啘,灏哖d閲戝睘钖勮啘涓嶴e绮夊皝鍦ㄩ珮鐪熺┖鐨勭煶鑻辩涓苟鍦ㄤ竴瀹氱殑娓╁害涓嬭繘琛岀鍖�,鑾峰緱PdSe₂钖勮啘銆傛牴鎹埅闈㈤珮鍒嗚鲸閫忓皠鐢甸暅锛圚RTEM锛夊浘鍍忓彲鐭dSe₂钖勮啘鐨勫钩鍧囧帤搴︾害涓�30 nm銆傝繘涓�姝ョ爺绌剁鍖栨俯搴﹀PdSe₂钖勮啘鐢佃緭杩愭�ц兘鐨勫奖鍝�,褰撶鍖栨俯搴︿负300鈩冩椂,鎵�鍒跺緱鐨凱dSe₂钖勮啘鐨勪綋绌虹┐娴撳害绾︿负1×10¹⁸ cm^-3,鍏锋湁鏈�澶х殑瀹ゆ俯杩佺Щ鐜囧拰瀹ゆ俯纾侀樆,鍒嗗埆涓�48.5 cm²·V^-1·s^-1鍜�12%(B=9T)銆傚�煎緱娉ㄦ剰鐨勬槸,鏈疄楠屼腑閫氳繃鐪熺┖纭掑寲娉曡幏寰楃殑钖勮啘绌虹┐杩佺Щ鐜囦紭浜庨�氳繃鏈烘鍓ョ娉曞埗寰楃殑p鍨婸dSe₂钖勮啘鐨勮縼绉荤巼銆傞殢鐫�纭掑寲娓╁害浠�300鈩冮�愭笎鍗囬珮,鐢变簬Se鍏冪礌瀹规槗鎸ュ彂,Pd钖勮啘鐨勭鍖栫▼搴﹂�愭笎鍑忓皬,瀵艰嚧钖勮啘纭掑惈閲忋�佽縼绉荤巼鍜岀鐢甸樆闄嶄綆銆傛湰鐮旂┒琛ㄦ槑锛氱湡绌虹鍖栨硶鏄竴绉嶇畝鍗曘�佹湁鏁堢殑鍒跺PdSe₂钖勮啘鐨勬柟娉�,鍦ㄨ吹閲戝睘纭棌鍖栧悎鐗╃殑澶ч潰绉埗澶囧強澶氬姛鑳界數瀛愬櫒浠剁殑璁捐涓叿鏈夋綔鍦ㄧ殑搴旂敤浠峰�笺�俔]> http://www.jim.org.cn/CN/10.15541/jim20200538 3Sb₂鍖栧悎鐗╁叿鏈夎壇濂界殑鐑數鎬ц兘鍜屾垚鏈紭鍔�,鍙楀埌浜嗙爺绌惰�呯殑骞挎硾鍏虫敞銆傜敱浜嶮g鍏冪礌鍏锋湁寰堥珮鐨勯ケ鍜岃捀姹藉帇鍜屽寲瀛﹀弽搴旀椿鎬�,鍥犳Mg₃Sb₂鍦ㄥ悎鎴愯繃绋嬩腑鍚噺闅句互绮剧‘鎺у埗銆傛湰鐮旂┒鍒╃敤鍥虹浉鍙嶅簲/鐞冪（缁撳悎鏀剧數绛夌瀛愪綋鐑х粨鍒跺浜嗕笉鍚孧g鍚噺鐨凪g_3(1+z)Sb₂锛�z=0,0.02,0.04,0.06鍜�0.08锛夋牱鍝�,閫氳繃鐗╃浉缁撴瀯鍒嗘瀽鍜岀儹鐢垫�ц兘娴嬭瘯,鐮旂┒浜哅g鍚噺瀵筂g₃Sb₂鍖栧悎鐗╃儹鐢垫�ц兘鐨勫奖鍝嶈寰嬨�傜粨鏋滆〃鏄�,闅忕潃鍚嶄箟Mg鍚噺鐨勫鍔�,瀹為檯Mg鍚噺鍦∕g₃Sb₂鍖栧悎鐗╀腑鐢辩己澶辩姸鎬佽浆鍙樹负杩囬噺鐘舵��,Mg_3(1+z)Sb₂锛�z=0,0.02,0.04锛夋牱鍝佸瓨鍦∕g绌轰綅锛�VMg鈥欌��锛�,琛ㄧ幇涓簆鍨嬩紶瀵�;鑰孧g_3(1+z)Sb₂锛�z=0.06,0.08锛夋牱鍝佷腑瀛樺湪闂撮殭Mg锛�Mgi路路锛�,琛ㄧ幇涓簄鍨嬩紶瀵笺�侻g_3(1+0.04)Sb₂鏍峰搧鍦ㄨ緝瀹芥俯鍖猴紙瀹ゆ俯鑷�770 K锛夊唴淇濇寔鏈�楂樼殑鐑數浼樺��,璇ユ牱鍝佹渶鎺ヨ繎鏈緛p鍨婱g₃Sb₂鍖栧悎鐗╃殑缁勬垚鍜岀儹鐢垫�ц兘銆傛湰鐮旂┒琛ㄦ槑,Mg鍚噺瀵筂g_3(1+z)Sb₂鍖栧悎鐗╄浇娴佸瓙绫诲瀷鍜屾祿搴︿互鍙婅縼绉荤巼鍏锋湁涓�瀹氱殑璋冩帶浣滅敤銆俔]> http://www.jim.org.cn/CN/10.15541/jim20200534 2姝ｆ瀬鏉愭枡涓�,瀵硅繃娓￠噾灞炲眰杩涜浜屽厓鍥烘憾鍙湁鏁堟彁鍗囩數鏋佹潗鏂欑殑鐢靛寲瀛︽�ц兘銆傛湰鐮旂┒鍒╃敤搴撲粦妯″瀷鏋勫缓浜哅g绂诲瓙鍥烘憾鐨凬a_x[Mg_1/3Mn_2/3]O₂缁撴瀯妯″瀷銆傞�氳繃绗竴鎬у師鐞嗚绠楀彂鐜�,鍦ㄩ挔绂诲瓙鍚噺灏忎簬2/3鏃�,Na_x[Mg_1/3Mn_2/3]O₂鐨勬斁鐢电數鍘嬭揪鍒�3.0V銆傜數瀛愭�佸瘑搴﹀拰鐢佃嵎甯冨眳鍒嗘瀽鍏卞悓琛ㄦ槑,Mg鐨勫浐婧舵縺娲讳簡P2鐩窷a_x[Mg_1/3Mn_2/3]O₂涓櫠鏍兼哀鐨勭數鍖栧娲绘��,浣夸綋绯荤殑鐢靛寲瀛﹀弽搴旀満鍒朵粠闃撮槼绂诲瓙鍗忓悓鐢靛寲瀛﹀弽搴旇浆鍙樹负鍙�嗛槾绂诲瓙鐢靛寲瀛﹀弽搴斻�傝繖涓�鏈虹悊涓洪挔绂诲瓙鐢垫睜鐢垫瀬鏉愭枡鐨勮璁℃彁渚涗簡涓�绉嶅叏鏂版柟娉�,涔熶负鍏跺畠绂诲瓙鐢垫睜鐨勪紭鍖栧拰鎺㈢储鎻愪緵浜嗗叏鏂扮殑鎬濊矾銆俔]> http://www.jim.org.cn/CN/10.15541/jim20200509 3娴撳害銆佸埢铓�鏃堕棿鍜屽埢铓�鐢垫祦瀵瑰鍚堢粨鏋勫舰璨岀殑褰卞搷瑙勫緥;娴嬭瘯浜嗛噰鐢ㄧ數鍌寲閲戝睘杈呭姪鍖栧鍒昏殌娉曞埗澶囨牱鍝佺殑鍦哄彂灏勭壒鎬с�傜粨鏋滄樉绀烘牱鍝佺殑闃堝�煎満寮轰负10.83 V/μm,褰撳満寮轰负14.16 V/μm鏃剁殑鐢垫祦瀵嗗害涓�64 μA/cm²銆俔]> http://www.jim.org.cn/CN/10.15541/jim20200475 Ф0.2×710 mm³鐨刌b³⁺鎺烘潅Y₃Al₅O₁₂(Yb:YAG)鍗曟櫠鍏夌氦,骞跺鍏惰繘琛屼簡琛ㄥ緛銆傚埗澶囩殑鍗曟櫠鍏夌氦闀垮緞姣斿ぇ浜�3500,鐩村緞娉㈠姩灏忎簬5%,涓旇〃鐜板嚭涓�瀹氱殑鏌旈煣鎬�;X灏勭嚎鎽囨憜鏇茬嚎娴嬭瘯缁撴灉鏄剧ずYb:YAG鍗曟櫠鍏夌氦鐨勭粨鏅惰川閲忎笌鎵�鐢ㄦ簮妫掔浉姣旀湁鎵�鎻愬崌;EDS绾挎壂鎻忕粨鏋滆瘉鏄庡崟鏅跺厜绾や腑鐨刌b³⁺娌胯酱鍚戝憟鐜板潎鍖�鍒嗗竷銆傚疄楠岀粨鏋滆〃鏄庯細鍑嗕竴缁村寲鐨勫崟鏅跺厜绾ゅ叿鏈夎壇濂界殑缁撴櫠璐ㄩ噺涓庡厜瀛﹀潎鍖�鎬�,鏈夋湜鎴愪负涓�绉嶆�ц兘浼樺紓鐨勯珮鍔熺巼婵�鍏夊鐩婃潗鏂欍�俔]> http://www.jim.org.cn/CN/10.15541/jim20200443 http://www.jim.org.cn/CN/10.15541/jim20200529 2SnC MAX鐩告潗鏂欍�傜粨鍚圶灏勭嚎琛嶅皠銆佹壂鎻忕數瀛愭樉寰暅鍜孹灏勭嚎鑳借氨绛夊垎鏋愭墜娈�,纭涓篠c₂SnC MAX鐨勭浉缁勬垚鍜屽井瑙傜粨鏋勩�傚苟閫氳繃瀵嗗害娉涘嚱鐞嗚璁＄畻浜哠c₂SnC MAX鐩哥殑缁撴瀯绋冲畾鎬с�佹櫠鏍煎弬鏁般�佸姏瀛﹀拰鐢靛瓙鎬ц川,鐞嗚璁＄畻缁撴灉琛ㄦ槑Sc₂SnC鐑姏瀛︾ǔ瀹�,Sc-3d鐢靛瓙鍦ㄨ垂绫宠兘绾т笂鍗犱富瀵煎湴浣�,MAX鐩稿憟閲戝睘鎬ц川銆俔]> http://www.jim.org.cn/CN/10.15541/jim20200506 -1锛夊閲戦粍鑹茶憽钀勭悆鑿屾湁鑹ソ鐨勬姂鍒舵�ц兘銆傚悓鏃�,鐢变簬閾滈捈绂诲瓙鐨勬嫯鎶椾綔鐢ㄨ兘闄嶄綆楂樻祿搴﹂摐绂诲瓙瀵圭粏鑳炵殑姣掓��,閽兼幒鏉傞摐纭呴挋鐭抽噴鏀剧殑閾滅瀛愬湪9.65 μg∙mL^-1鐨勯珮娴撳害涓嬩緷鐒惰兘淇濊瘉浜鸿剱闈欒剦鍐呯毊缁嗚優瀛樻椿鐜囬珮杈�90%銆傚洜姝�,閽兼幒鏉傚彲浠ヤ綔涓哄惈閾滅敓鐗╂潗鏂欓檷浣庡叾缁嗚優姣掓�х殑涓�绉嶆湁鏁堥�斿緞,涓哄紑鍙戜綆缁嗚優姣掓�у惈閾滄姉鑿岀敓鐗╂潗鏂欐彁渚涗簡鏂扮殑璺緞銆俔]> http://www.jim.org.cn/CN/10.15541/jim20200498 3?g^-1锛夊拰瀛斿緞鍒嗗竷鍔犲锛�0.5~60 nm锛夈�傚洜姝�,鑾峰緱鐨勫瘜姘幒鏉傜⒊鏉愭枡鍏锋湁302 F?g^-1@1 A?g^-1鐨勯珮瀹归噺鍜�177 F?g^-1@120 A?g^-1鐨勬澃鍑哄�嶇巼鎬ц兘銆傛鐙壒鐨勫浐姘柟娉曟槸涓�绉嶆湁娼滃姏鐨勫埗澶囬珮鎬ц兘瓒呯骇鐢靛鍣ㄧ數鏋佹潗鏂欑殑绛栫暐銆俔]> http://www.jim.org.cn/CN/10.15541/jim20200495 L-3-(4鍚″暥鍩�)-涓欐皑閰�(PLA))銆傛祴璇曠粨鏋滄樉绀篜LA鐨勫紩鍏ュ彲鎻愰珮鍣ㄤ欢鐨勫悇鍏夌數鎬ц兘鍙傛暟,鍚玃LA鍣ㄤ欢鐨勬渶浼樿兘閲忚浆鎹㈡晥鐜囦负21.53%,鑰屽弬鐓у櫒浠朵负20.10%銆傝繘涓�姝ョ爺绌惰〃鏄庡紩鍏LA鍙欢闀胯崸鍏夊鍛�,闄嶄綆鍣ㄤ欢鐨勯櫡闃辨�佸瘑搴�(浠�5.59 × 10¹⁶ cm^-3闄嶈嚦3.40 × 10¹⁶ cm^-3),淇冭繘鐣岄潰鐢佃嵎鎶藉彇,鎶戝埗杞芥祦瀛愬鍚堛�傚櫒浠舵�ц兘鐨勬彁鍗囨槸鐢变簬PLA瀵艰嚧鐨勯挋閽涚熆钖勮啘鏅剁晫澶凱bI₂鐨勫瘜闆嗗強PLA鍦ㄧ晫闈㈠鐨勯敋瀹氳捣鍒颁簡閽濆寲缂洪櫡鐨勪綔鐢ㄣ�傛湰鐮旂┒鍙互涓鸿繘涓�姝ヨ皟鎺ч挋閽涚熆澶槼鐢垫睜鐨勭己闄锋彁渚涘�熼壌銆俔]> http://www.jim.org.cn/CN/10.15541/jim20200450 -1鏃�,鎭掓俯35 鈩冧笅鏂介晙1 h,鍒跺鐨凬d-Ni-B/NF鐢垫瀬鏋愭阿鎬ц兘鏈�浣炽��1.0 mol∙L^-1KOH 婧舵恫涓�,Nd-Ni-B/NF鐢垫瀬鍦�20 mA∙cm^-2涓嬬殑鏋愭阿杩囩數浣嶄粎涓�180 mV,Tafel鏂滅巼涓�117 mV∙dec^-1,鏋愭阿鍙嶅簲鐢盫olmer-Heyrovsky姝ラ鎺у埗銆傛澶�,Nd-Ni-B/NF鐢垫瀬鍏锋湁浼樿秺鐨勭數鍖栧绋冲畾鎬�,鍦ㄦ寔缁數瑙�12 h鎴�2000娆″惊鐜紡瀹夋祴璇曞悗,鍌寲鍓傜殑娲绘�ф病鏈夋槑鏄捐“鍑忋�俔]> http://www.jim.org.cn/CN/10.15541/jim20200440 _xHf_1-xC鍥烘憾闄剁摲鏄⒊鍖栭捊锛圱aC锛夊拰纰冲寲閾紙HfC锛夊湪涓�瀹氭潯浠朵笅褰㈡垚鐨勫浐婧朵綋,鍏剁啍鐐瑰彲杈�4300 K浠ヤ笂,涓旂‖搴﹂珮銆佹ā閲忛珮銆佺儹瀵肩巼浣庛�佹姉楂樻俯姘у寲鍜屾姉鐑ц殌鎬ц兘浼樺紓,鍏峰鍦ㄦ瀬绔儹鐜锛�>3000 K锛変笅鏈嶅焦鐨勬綔鍔�,鎴愪负鑰愯秴楂樻俯鏉愭枡棰嗗煙鐨勭爺绌剁儹鐐瑰拰鍓嶆部銆傛湰鏂囩患杩颁簡杩戝勾鏉a_xHf_1-xC鍥烘憾闄剁摲鍦ㄥ埗澶囧伐鑹恒�佺粍鎴愮粨鏋勫強鐗╃悊鍖栧鎬ц兘绛夋柟闈㈡墍鍙栧緱鐨勭爺绌惰繘灞�,璁ㄨ浜員a_xHf_1-xC鍥烘憾闄剁摲缁勬垚銆佺粨鏋勪笌鎬ц兘涔嬮棿鐨勭浉浜掑叧绯�,鏈�鍚庡睍鏈涗簡Ta_xHf_1-xC鍥烘憾闄剁摲鐨勬綔鍦ㄥ彂灞曟柟鍚戙�俔]> http://www.jim.org.cn/CN/10.15541/jim20200404 http://www.jim.org.cn/CN/10.15541/jim20200356 5O₇I寮傝川缁撳鍚堝厜鍌寲鏉愭枡銆備笌绾疊i₅O₇I寰背妫掑強绾疌uS鏍峰搧鐩告瘮锛孋uS/Bi₅O₇I澶嶅悎鍌寲鍓傚Cr(VI)姘存憾娑插叿鏈夋洿楂樼殑鍏夊偓鍖栭檷瑙ｆ椿鎬с�傚湪鐩稿悓鐨勫彲瑙佸厜杈愮収鏉′欢涓嬶紝15wt%CuS淇グ鐨勫鍚堟牱鍝侊紝鍏夊偓鍖栭檷瑙r(VI)鐨勫弽搴斿父鏁版槸绾�/Bi₅O₇I鏍峰搧鐨�20鍊嶏紝鏄函CuS鏍峰搧鐨�4.3鍊嶃�傚姣旀牱鍝佺殑姣旇〃闈㈢Н銆佸厜鑷村彂鍏夎氨鍜岀數鍖栧闃绘姉璋辩殑娴嬭瘯缁撴灉锛屽彂鐜板鍚堟牱鍝佽〃鐜板嚭鏇撮珮鐨勫偓鍖栨晥鐜囨槸鐢变簬CuS/Bi₅O₇I鍏锋湁鏇村ぇ鐨勬瘮琛ㄩ潰绉�佹洿瀹界殑鍏夊惛鏀跺尯鍩熷強鏇撮珮鐨勫厜鐢熺數瀛�-绌虹┐瀵圭殑鍒嗙鍜屼紶杈撴晥鐜囥�傝鏂囪繕鎻愬嚭浜咰uS/Bi₅O₇I澶嶅悎鏉愭枡鍏夊偓鍖栭檷瑙r(VI)鐨勬満鐞嗐�俔]> http://www.jim.org.cn/CN/10.15541/jim20200508 2O₃/Er₃Al₅O₁₂(ErAG)鍜孉l₂O₃/Yb₃Al₅O₁₂(YbAG) 瀹氬悜鍑濆浐鍏辨櫠闄剁摲銆傚湪10 mm/h鐨勬娊鎷夐�熺巼涓嬫垚鍔熻幏寰椾簡鍑濆浐缁勭粐鍧囧寑銆佸唴閮ㄦ棤瑁傜汗鎴栧瓟娲炵殑楂樿川閲忓叡鏅堕櫠鐡枫�傞�氳繃楂樺垎杈ㄤ笁缁碭灏勭嚎琛嶅皠浠爺绌朵簡Al₂O₃鍜孯E₃Al₅O₁₂鍦ㄤ笁缁寸┖闂寸殑鍒嗗竷涓庣粍缁囩粨鏋�;鍒╃敤鐢靛瓙鑳屾暎灏勮灏勬妧鏈垎鏋愪簡瀹氬悜鍑濆浐鏈湡Al₂O₃鍜孯E₃Al₅O₁₂涓ょ浉鐨勬櫠浣撳鎷╀紭鍙栧悜鍜岀浉鐣岄潰鍏崇郴銆傚姏瀛︽�ц兘琛ㄥ緛缁撴灉鏄剧ず,Al₂O₃/ErAG鍜孉l₂O₃/YbAG鍏锋湁浼樺紓鐨勫姏瀛︽�ц兘,浜岃�呯殑缁存皬纭害鍒嗗埆涓猴紙13.5±0.4锛夊拰锛�12.8±0.1锛� GPa;鏂闊ф�у垎鍒负锛�3.0±0.2锛� MPa·m^1/2鍜岋紙3.2±0.1锛� MPa·m^1/2銆俔]> http://www.jim.org.cn/CN/10.15541/jim20200499 http://www.jim.org.cn/CN/10.15541/jim20200484 2+娴撳害銆傜爺绌朵簡涓嶅悓SBF婧舵恫涓瑽BG楠ㄦ按娉ヨ〃闈㈠舰鎴愮殑鐭垮寲浜х墿銆傜爺绌剁粨鏋滆〃鏄�,涓嶅悓鐨勬皑鍩洪吀鍙婃祿搴︾殑鍙樺寲瀵圭熆鍖栦骇鐗╃殑褰卞搷鏈夎緝澶у樊寮�,澶╁啲姘ㄩ吀鍜岃禆姘ㄩ吀鐨勬祿搴﹀彉鍖栧奖鍝嶇熆鐗╃殑闀垮緞姣�,鑰岀敇姘ㄩ吀瀵圭熆鐗╁舰璨岀殑褰卞搷杈冨皬銆傚皢纭肩閰哥洂鐢熺墿娲绘�х幓鐠冨帇鐗囨斁缃湪70鈩冧笅鐨勯珮Mg²⁺娴撳害鐨勯吀鎬э紙pH=3.5锛塖BF婧舵恫涓蹈娉′竴瀹氭椂闂村悗,鑳藉鑾峰緱HA/WH鐨勫鐩哥熆鐗┿�俔]> http://www.jim.org.cn/CN/10.15541/jim20200361 http://www.jim.org.cn/CN/10.15541/jim20200357 0.4Zr_0.5La_0.05Pr_0.05O₂锛圥t/CZ锛変笁鏁堝偓鍖栧墏,鍒嗘瀽浜嗕笉鍚岀⒈瀵瑰偓鍖栧墏鐗╃悊鍖栧鎬ц川銆佸偓鍖栨椿鎬у拰鑰愪箙鎬х殑褰卞搷銆傜粨鏋滆〃鏄�,灏跨礌杈呭姪娌夌Н娌夋穩娉曪紙UDP锛夊埗澶囩殑Pt/CZ鍌寲鍓傜殑鎶楄�佸寲鎬ц兘杈冨樊,鑰屾皑姘磋緟鍔╂矇绉矇娣�娉曪紙ADP锛夊埗澶囩殑鍌寲鍓傜殑鎶楄�佸寲鑳藉姏杈冨己銆俋RD,CO鍚搁檮,XPS鍜孒₂-TPR琛ㄥ緛缁撴灉琛ㄦ槑ADP涓緝澶х殑Pt棰楃矑浠ュ強鏇村己鐨勯噾灞炶浇浣撶浉浜掍綔鐢ㄤ娇ADP鍦ㄨ�佸寲杩囩▼涓儳缁撶▼搴﹁緝杞�,鏈夊埄浜庣淮鎸佸偓鍖栨椿鎬с�傚洜姝�,ADP鍌寲鍓傚叿鏈変竴瀹氱殑宸ヤ笟搴旂敤鍓嶆櫙銆俔]> http://www.jim.org.cn/CN/10.15541/jim0200396 K_m鍒嗗埆涓�0.109鍜�0.083,瀵瑰簳鐗╁叿鏈夎壇濂界殑浜插拰鑳藉姏;N-HCSs姘у寲鐗╂ā鎷熼叾鍌寲鍙嶅簲涓捣涓昏浣滅敤鐨勬椿鎬ф哀鍩哄洟鏄秴姘ч槾绂诲瓙锛圤₂•^-锛夈�傛湰鐮旂┒涓洪珮娲绘�ф棤鏈洪潪閲戝睘绫绘哀鍖栫墿妯℃嫙閰剁殑璁捐鍜屽埗澶囨彁渚涗簡鐞嗚渚濇嵁銆俔]> http://www.jim.org.cn/CN/10.15541/jim20200347 http://www.jim.org.cn/CN/10.15541/jim20200266